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  • Physics  (107)
  • Cell & Developmental Biology
  • 1980-1984
  • 1975-1979  (66)
  • 1970-1974  (76)
  • 1960-1964
  • 1950-1954
  • 1975  (66)
  • 1971  (76)
Collection
Keywords
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  • 1980-1984
  • 1975-1979  (66)
  • 1970-1974  (76)
  • 1960-1964
  • 1950-1954
Year
  • 1
    Electronic Resource
    Electronic Resource
    Crystallization of polyethylene at elevated pressures (1971)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A-2: Polymer Physics 9 (1971), S. 385-406 
    Details
    ISSN: 0449-2978
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The crystallization from the melt of three sharp polyethylene fractions has been studied at 5 kbar. It has been shown that the thickness of so-called extended-chain lamellae is a function of time, temperature, and molecular weight. There is by no means just the fully extended molecular configuration present. Crystallization is qualitatively similar to that of chain-folded crystals at 1 bar, giving an optimum lamellar thickness which increases with time and decreasing supercooling. Fractional crystallization is widespread and is a major cause of disparate lamellar thickness. Isothermal thickening of lamellae during crystallization has been established directly. Morphological detail suggests further that layers can increase their thickness tenfold over their initial size.
    Additional Material: 14 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1971.160090301
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  • 2
    Electronic Resource
    Electronic Resource
    Nuclear magnetic resonance study of rubber-carbon black interactions (1971)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A-2: Polymer Physics 9 (1971), S. 829-839 
    Details
    ISSN: 0449-2978
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The mobilities of polymer chain segments in mixtures of rubber and carbon black were investigated by nuclear magnetic resonance. Spin-spin relaxation time (T2) measurements on cis-polybutadiene and ethylene-propylene-diene rubber (EPDM) bound rubbers detected at least two relaxing regions: an immobile region and a relatively free region. The molecular motions in the relatively free region are still constrained compared to those of the pure gum.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1971.160090505
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  • 3
    Electronic Resource
    Electronic Resource
    RNA metabolism in thoracic duct lymphocytes from thymectomized ratsSupported by grant IC-18A from the American Cancer Society, grant AI-08642 from the National Institute of Allergy and Infectious Diseases. (1971)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Cellular Physiology 78 (1971), S. 465-467 
    Details
    ISSN: 0021-9541
    Keywords: Life and Medical Sciences ; Cell & Developmental Biology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Biology , Medicine
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jcp.1040780316
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  • 4
    Electronic Resource
    Electronic Resource
    Nuclear spin relaxation in poly(diethylsiloxane) (1975)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 13 (1975), S. 1269-1274 
    Details
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Earlier work showed that heating causes poly(diethylsiloxane) to undergo a first-order transition from a semicrystalline solid to a more mobile viscous - crystalline material. The latter is composed of two phases and analogies between polymer and liquid crystal morphology and behavior have been made. The viscous - crystalline phase in PDES appears to be unique since the literature is devoid of other documented examples. In this study, spin - lattice and spin - spin relaxation times were measured over a wide temperature range. They show a glass transition at 138°K, a crystal - crystal transition at 206°K, and a transition around 250°K which results from translational motion of the polymer chains with respect to each other. This motion is observed in the amorphous phase at a lower temperature than in the crystalline phase. Translational motion in the crystalline phase is observed on melting of the crystallites. The spin - spin data permitted monitoring of the molecular motions in each phase and the data suggest that these phases exert some influence on the molecular motions of each other. The viscous - crystalline phase in PDES may represent a unique model for studying and understanding “precrystalline” behavior and structure in amorphous solids.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1975.180130701
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  • 5
    Electronic Resource
    Electronic Resource
    Driving force for hydraulic and pervaporative transport in homogeneous membranes (1975)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 13 (1975), S. 1201-1214 
    Details
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Experiments were designed to demonstrate that the chemical potential gradient required for liquid transport through swollen network polymer membranes manifests itself as a concentration gradient and that the rate of transport is independent of how this gradient is established. The fluxes of various liquids through a crosslinked rubber membrane were measured in hydraulic and pervaporation modes of permeation. The pressure applied downstream in the latter act simply to fix the activity of the liquid in the downstream membrane surface. The experiments show the flux is a unique function of this activity, and it does not matter how it is established. Sorption data were used to convert these results into a plot of flux versus concentration differential across the membrane which was analyzed by Fick's law using a model for the concentration dependence of the diffusion coefficient. Measured ceiling fluxes for pervaporation for a number of liquids were found to be the same as those estimated from hydraulic permeation data. A simple mathematical representation for an ideal system is used as a pedagogical device to demonstrate the conclusions.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1975.180130612
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  • 6
    Electronic Resource
    Electronic Resource
    The elongation and time dependence of the crystallinity of low-density polyethylene (1975)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 13 (1975), S. 1945-1957 
    Details
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: It has been presumed in studies of the orientation of low-density polyethylene and its time dependence that the degree of crystallinity remained constant with elongation and did not vary with time following elongation. This paper represents a test of this hypothesis by several methods. The change in crystallinity accompanying stretching has been followed by a modification of an x-ray method for uniaxial orientation proposed by Ruland in which diffraction peaks are resolved into crystalline and amorphous components and their respective areas are determined by two-dimensional integration over both the Bragg angle and the azimuthal angle of diffraction. The weight-fraction crystallinity is then determined from the ratio of the weighted crystalline area to the total area. There appears to be no significant variation in crystallinity up to 50% sample elongation for both slowly and rapidly stretched samples at room temperature. The dynamic crystallinity change accompanying small amplitude vibration has also been determined by the dynamic x-ray diffraction technique and found to be negligible over a wide range of frequency. The degree of crystallinity has also been evaluated from the absolute infrared absorbance of crystallinity-sensitive bands and has also been found to be independent of elongation at room temperature up to 80% elongation. Changes have also been observed by this method during relaxation at constant length following rapid extension and have also been found to be negligible. These results also indicate negligible changes in rotational isomer population. Consequently, we conclude that changes observed during relaxation and vibration arise from orientational changes rather than changes in the degree of crystallinity.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1975.180131009
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  • 7
    Electronic Resource
    Electronic Resource
    Dielectric study of relaxations and polymorphism in poly(diethyl siloxane) (1975)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 13 (1975), S. 977-983 
    Details
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The dielectric behavior of poly(diethyl siloxane) supports the adiabatic calorimetric findings of Beatty and Karasz. In particular, a sub-Tg transition is observed near -180°C at 100 Hz, the glass transition near -135°C at 100 Hz, and a first-order transition near -70°C (crystal-crystal transformation). This glass-transition temperature is the lowest reported polymeric glass transition for polymers.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1975.180130510
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  • 8
    Electronic Resource
    Electronic Resource
    13C NMR of polybutadienes (1975)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Chemistry Edition 13 (1975), S. 1963-1967 
    Details
    ISSN: 0360-6376
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 4 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1975.170130822
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  • 9
    Electronic Resource
    Electronic Resource
    Preparation of films exhibiting a balanced temperature dependence to permeation by aqueous solutions - a study of lower consolute behavior (1975)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Chemistry Edition 13 (1975), S. 2551-2570 
    Details
    ISSN: 0360-6376
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Temperature dependence of solute transport through aqueously swollen polymeric films and membranes can be altered to show even apparent negative activation energies by the use of polymers exhibiting a lower consolute behavior in solution. The principles by which we constructed a host of such polymers are discussed. A solubility rule is presented which predicts that solutes in water will show a lower critical solution temperature if the proper hydrophilic-hydrophobic balance is achieved.
    Additional Material: 19 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1975.170131113
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  • 10
    Electronic Resource
    Electronic Resource
    Polymerization of the N-carboxy anhydrides of alloisoleucinePresented to the International Symposium on Macromolecular Chemistry, Budapest, Hungary, 1969. (1971)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A-1: Polymer Chemistry 9 (1971), S. 2079-2083 
    Details
    ISSN: 0449-296X
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1971.150090724
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