ISSN:
1612-1112
Schlagwort(e):
Aniline
;
Dimethylthiophosphinyl derivatives
;
Mass fragmentography
;
Environmental analysis
Quelle:
Springer Online Journal Archives 1860-2000
Thema:
Chemie und Pharmazie
Notizen:
Summary A method for trace analysis of aniline in water, urine and serum samples is presented. Internal standardisation with d5-aniline, extraction, derivatisation with dimethylthiophosphinic chloride, gas chromatographic separation on a glass capillary column and mass fragmentographic quantitation are essential steps of the analytical procedure. A detection limit of 20 pg/ml in water and 500 pg/ml in urine or serum is achieved.
Materialart:
Digitale Medien
URL:
http://dx.doi.org/10.1007/BF02258896
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