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Synthese neuer N, N,1,1-Tetramethyl-isobenzofuranamine (1993)

Stanetty, Peter ; Rodler, Inge ; Krumpak, Barbara

New York, NY : Wiley-Blackwell

Journal für Praktische Chemie/Chemiker-Zeitung 335 (1993), S. 17-22

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ISSN: 0941-1216

Keywords: Chemistry ; Organic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Synthesis of New N, N,1,1-Tetramethyl-isobenzofuranaminesThe nitrophthalides 3a-d aimed as intermediates in the synthesis of the title compounds 6a-d were obtained via regioselective reduction of 3-nitrophthalic anhydride 1 or by nitration of phthalide and 3,3-dimethylphthalide, respectively. Reductive methylation of the nitro groups afforded the dimethylaminophthalides 5a-d which in turn were reacted with MeMgI or in the case of 5d reduced by LiAlH4 leading finally to the title compounds.

Additional Material: 1 Tab.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/prac.19933350104

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