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  • American Physical Society (APS)
  • International Union of Crystallography (IUCr)
  • 1990-1994  (7,163)
  • 1955-1959  (1,463)
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  • 1
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 18-20 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Anomalous X-ray scattering terms for Rb+ near the K-edge measured in diffraction experiments with synchrotron radiation range up to 4.71 (6) for f′′ and down to −9.80 (11) for f′, in agreement with values derived from the absorption spectrum.
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  • 2
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 35-42 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: The X-ray reflectivity of bent perfect crystals is calculated from a model where the crystal is approximated by a stack of perfect-crystal lamellae which have a gradually changing orientation. A computer program is developed for calculation of the reflectivity of the composite crystal from the dynamical theory of diffraction. An approximate solution is also given where an analytical formula for the reflectivity of a non-absorbing lamella is used and the effects of absorption are calculated separately. Typically, in the Bragg case, the reflectivity curve has a steep edge and an exponentially falling slope, while in the Laue case the curve is almost rectangular if the absorption is not too large. The width of the curve is inversely proportional to the bending radius in both cases. Reflectivity curves were measured for the 111 and 400 reflections of Si with Mo Kα1 radiation. The agreement with analytical and computer calculations is good, particularly at small bending radii where the kinematical limit is approached.
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  • 3
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 63-69 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: A method of measuring differences in lattice spacing with an accuracy of 1 part in 108 in a period as short as two minutes is described. The method uses one source of copper radiation and a triple-axis arrangement. Two of these axes are double-leaf silicon springs in monolithic crystal assemblies which achieve the high stability required by such measurements. Samples are easily changed and sequences of measurements are performed entirely under computer control. The method is demonstrated by a comparison of the lattice spacings of four samples which reveals differences of up to 60 parts in 108 between silicon crystals of different origins.
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  • 4
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 77-78 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
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  • 5
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 105-110 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Some experimental results are presented for an elastically bent perfect silicon crystal in a strongly asymmetric diffraction geometry as a neutron monochromator. The use of this unconventional geometry of the monochromator appears to be suitable for a wide (several centimetres) incident polychromatic beam, when, thanks to the spatial condensation of the diffracted neutrons (Fankuchen effect), a high monochromatic beam density may be obtained. Furthermore, when using focusing in real and in momentum space by adjusting an optimum bending radius, the intensity diffracted by a sample may be comparable even with the best mosaic monochromators such as highly oriented pyrolytic graphite (PG). A comparison is demonstrated on the rocking curves of a strongly mosaic Ni–Al(020) crystal obtained with the monochromatic beam from bent Si(111), Si(400) and from PG(002), Cu(220) mosaic monochromators.
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  • 6
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 134-135 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Bhatia & Thornton [Phys. Rev. B. (1970), 2, 3004–3012] have derived the formula that relates the scattering intensity of a binary system to the Fourier transform of the local number density and concentration. For the intensity at the limit of zero scattering angle, the same formula can be derived by a much simpler process.
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  • 7
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 142-143 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
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  • 8
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 144-146 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
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  • 9
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 169-174 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Single-crystal synchrotron-radiation Laue photographs of protein crystals and viruses are densely populated and a considerable amount of spatial overlapping of spots often occurs on the films. An integration procedure which enables the efficient deconvolution of these spots in order to obtain their integrated intensity has been developed and implemented. Some results are given for glycogen phosphorylase b and tomato bushy stunt virus. A comparative study of reflections overlapped on one exposure and separated on another, taken from the same crystal at a longer crystal-to-film distance, gives merging statistics comparable to those from the treatment of spatially separated spots only. In all cases the majority of the spatially overlapped data is made available for subsequent analyses.
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  • 10
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 23 (1990), S. 211-212 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Previous reports by Rosenzweig & Morosin [Acta Cryst. (1966). 20, 758–761], Liminga & Abrahams [J. Appl. Cryst. (1976). 9, 42–47] and Svensson, Albertsson, Liminga, Kvick & Abrahams [J. Chem. Phys. (1983). 78, 7343–7352], that the more steeply pointed ends of α-LiIO3 crystals grown from aqueous solution with 3 ≤ pH ≤ 7 have the apex of each pyramidal IO−3 ion pointing toward the direction which develops a positive polarity (d33 〉 0) under tensile stress applied along the polar hexagonal axis, have been confirmed contrary to the conclusion of Yang Hua-guang, Zhang Dao-fan, Chen Wan-chun & Li Yin-yuan [J. Appl. Cryst.(1989). 22, 144–149]. The error leading to the latter conclusion is identified.
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