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  • 1
    Electronic Resource
    Electronic Resource
    Synthesis and Investigations on Nitrido(phthalocyaninato)rhenium Complexes (1999)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 1999 (1999), S. 1309-1313 
    Details
    ISSN: 1434-1948
    Keywords: Phthalocyanines ; Rhenium ; Nitrido(octa-n-alkylphthalocyaninato)rhenium compounds ; Nucleophilic additions ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The reactions of nitrido(tetra-tert-butylphthalocyaninato)rhenium (1) with boron tribromide leading to (tBu4Pc)ReNBBr3 (4) and with acetone to give the imido complex (tBu4Pc)Re[NC(CH3)2CH2C(O)CH3]OH (2b) and its μ-oxo dimer 3 are reported. Starting from the corresponding 4,5-di-n-alkylphthalonitriles and ammonium perrhenate four soluble nitrido(octa-n-alkylphthalocyaninato)rhenium complexes 5-8 were synthesized. Nitrido(octa-n-pentylphthalocyaninato)rhenium (6) was treated with boron tribromide to afford [(C5H11)8Pc]ReNBBr3 (9).
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
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    Paper (German National Licenses)
  • 2
    Electronic Resource
    Electronic Resource
    Novel Nitrido- and Oxo(phthalocyaninato) Complexes of Molybdenum, Tungsten and Rhenium (2000)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 2000 (2000), S. 1025-1030 
    Details
    ISSN: 1434-1948
    Keywords: Phthalocyanines ; Nitrides ; Oxo complexes ; Rhenium ; Molybdenum ; Tungsten ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The synthesis of new nitrido(phthalocyaninato)molybdenum (1-4) and -tungsten complexes (5-7) starting from the corresponding phthalonitriles and MNCl3 (M = Mo, W) is reported. In addition, the reaction of (tBu4Pc)WN (6) with PPh3 leading, after several steps, to the diamagnetic compound (tBu4Pc)WO (7) is described. The reaction of (tBu4Pc)ReN (9) with PPh3 leads to [(tBu4Pc)ReO]2 (12), and of [(C5H11)8Pc]ReN (10) with PPh3 leads, under different conditions, to {[(C5H11)8Pc]ReO}2O (11).
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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    Paper (German National Licenses)
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