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Beryllium-tetrakis-[trimethylsilyl]-diamid-eine Verbindung mit zweibindigem Beryllium (1965)

Bürger, H. ; Forker, Christine ; Goubeau, J.

Springer

Monatshefte für Chemie 96 (1965), S. 597-601

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ISSN: 1434-4475

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Description / Table of Contents: Abstract Monomeric I has been prepared (yield 68%) by the reaction of BeCl2 with NaN[Si(CH3)3]2 in ether. Properties, infrared, raman and1H-NMR-spectra support a NBeN angle of 180°. SiN and BeN force constants were calculated to be 3,40 and 2,96 mdyn/Å, respectively.

Notes: Abstract Monomeres [(CH3)3Si]2NBeN[Si(CH3)3]2 (I) entsteht in 68% Ausb. bei der Reaktion von BeCl2-Ätherat mit NaN[Si(CH3)3]2. Eigenschaften, IR-, Raman- und1H-NMR-Spektren sprechen für einen NBeN-Winkel von 180°. Die SiN- und BeN-Valenzkraftkonstanten werden zu 3,40 bzw. 2,96 mdyn/Å errechnet.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00909476

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