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Preparation, characterization and crystal structure of Na4[Mn(NCS)6]·13H2O (1997)

Böhland, Heinz ; Härtung, Helmut ; Baumeister, Ute ; [et al.]

Springer

Microchimica acta 125 (1997), S. 149-152

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ISSN: 1436-5073

Keywords: hexaisothiocyanatomanganate(II) ; X-ray structure analysis ; magnetic susceptibility ; dehydration reactions

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract Na4[Mn(NCS)6] · 13H2O was prepared and characterized by chemical analysis, magnetic susceptibility, thermal dehydration reactions, and single crystal X-ray structure analysis. The crystals are triclinic with a=9.310(1)Å, b=9.367(1)Å, c=9.730(2)Å, α= 89.89(1)°,β=75.33(1)°, γ=70.72(1)°, space group P¯I.Z=1. The structure is built up from Na(H2O)5 S, Na(H2O)6, and Mn(NCS)6, octahedra. All water molecules are coordinated to Na+ -ions in terminal as well as bridging fashion. They form O-H···O as well as O-H···S hydrogen bonds.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01246178

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