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Conversion process of chlorine containing polysilanes into silicon carbide (1996)

Martin, H. P. ; Müller, E. ; Brendler, E.

Springer

Journal of materials science 31 (1996), S. 4363-4368

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ISSN: 1573-4803

Source: Springer Online Journal Archives 1860-2000

Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics

Notes: Abstract The crystallization of pyrolysed chlorine containing polycarbosilanes (PCS) into silicon carbide is suggested to begin at about 1000 °C by X-ray diffraction experiments. The crystallite size and the crystallite amount were also estimated from the X-ray diffraction patterns. Electron spin resonance, nuclear magnetic resonance and Raman-spectroscopy were used to describe the structure of the material. In addition to these methods a combustion method was used to investigate the carbon and the oxygen contents.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00356461

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