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Preparation of spherical zirconium salt particles by homogeneous precipitation (1995)

Shi, J. L. ; Gao, J. H.

Springer

Journal of materials science 30 (1995), S. 793-799

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ISSN: 1573-4803

Source: Springer Online Journal Archives 1860-2000

Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics

Notes: Abstract Spherical basic zirconium sulphate particles were prepared by homogeneous precipitation in mixed solutions of zirconium sulphate and urea. Values of [SO 4 2− ]/[Zr4+] and [urea]/[Zr4+] in starting mixed solutions and cooling rate may affect the formation of spherical particles. Complexes such as [Zr(OH)n]4−n could prevent the formation and thus lead to gel precipitation. In addition, spherical particles could only be obtained in the presence of SO 4 2− ; for NO3− and Cl−, only gel precipitation occurred.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00356344

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