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  • 1
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 623 (1997), S. 1040-1042 
    ISSN: 0044-2313
    Keywords: 2,2′,3,3′,4,4′-hexatertiarybutyl-1,1′-bicyclotetraarsane ; arsenic polycycles ; structural isomers ; crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: tBu6As8 - a Compound of Known Composition and New StructureThe compound 2,2′,3,3′,4,4′-hexatertiarybutyl-1,1′-bicyclotetraarsane (1) can be obtained in good yields through the reaction of (tBuAs)4 with [Co2(CO)8]. 1 is the structural isomer of 2,3,4,6,7,8-hexatertiarybutylbicyclo-[3.3.0]octaarsane (2) described in 1981 by Baudler et al. [3]. 1 was characterized by 1H-NMR spectroscopy, mass spectroscopy and crystal structure analysis. Isomerisation into 2 can be observed, by tempering a solution of 1 in toluene for ten hours at 90°C.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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