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  • 1
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Contributions to the Chemistry of Sulfur. 115. Crystal and Molecular Structure of BenzopentathiepineThe structure of benzopentathiepine has been determined from three-dimensional single-crystal X-ray data. The crystal are monoclinic, space group P21/c, with 4 molecules in the unit cell of dimensions a = 6.942(4) Å, b = 10.223(10) Å, c = 13.015(8) Å, β = 102,15(10)°. The conformation of the seven-membered ring is the chair form. Details of the conformation are discussed. Bond distances, bond angles, and dihedral angles are compared with those in other molecules, which have similar structure.
    Notes: Die Struktur von Benzopentathiepin wurde aus Einkristalldaten röntgenographisch bestimmt. Die Kristalle sind monoklin, Raumgruppe P21/c, mit 4 Molekeln in der Elementarzelle. Die Gitterkonstanten sind: a = 6,942(4) Å, b = 10,223(10) Å, c = 13,015(8) Å, β = 102,15(10)°. Der siebengliedrige Ring liegt in der Sesselkonformation vor. Einzelheiten der Konformation werden diskutiert. Bindungslängen und -winkel sowie die Diederwinkel werden mit denen anderer Molekeln ähnlicher Struktur verglichen.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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