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  • 1
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Chemistry of Silicon-Nitrogen Compounds. CXXXI. 1,2-Bis (organylamino) - tetramethyldisilaries and their Transformation into N,N′-Bis (organyl) octamethyltetrasiladiaza-cyclohexanes1,2-Bis(organylamino)disilanes A 1-4 were prepared via equ. 3 by aminolysis of 1,2-dichlorotetramethyldisilane and transformed by three different methods (equ. 7; 8/9 and 10/11) into the N,N′ variied tetrasiladiazacyclohexanes B 2-5. Physical, analytical and structural information can be taken from tables 1-3. The bond increments (N)Si—Si(N) of the EISENLOHR molar refractions MRE were reinvestigated with 24.5 instead of 30.0.
    Notes: Organylaminolyse des 1,2-Dichlortetramethyldisilans führt nach Rk. 3 zu den entsprechenden 1,2-Bis(organylamino)-Derivaten A 1-4. Sie ließen sich auf 3 verschiedenen Wegen (Rkk, 7, 8/9 bzw. 10/11) in die N,N′-variierten Tetrasiladiazacyclohexane B 2-5 überführen. Physikalische, analytische und strukturelle Daten der neu dargestellten Verbindungen finden sich in Tab. 1-3. Das Bindungsinkrement (N)Si-Si(N) für die Molrefraktionen MRE nach EISENLOHR wurde neu bestimmt zu 24,5, bisher 30,0.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
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