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  • 1
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the „HCl- Condensation“ of Phosphorus OxytriamideThe reaction of HCl with phosphorus oxytriamide suspended in ether leads to highly cross-linked imidopolyphosphates. By substitution of amido group by chlorine atoms amidochlorides of phosphoric acid are also formed which are soluble in ether. Only traces of oligomeric μ-imidophosphoric acid amides are obtained. The intermediate formation of phosphorylimide amide, OP(=NH)NH2, and phosphoryl imide chloride, OP(=NH)CI, is assumed to explain the experimental results.
    Notes: Die Reaktion von HCl mit Phosphoroxidtrimid in ätherischer Suspension führt zur Bildung stark vernetzter Imidopolyphosphate. Durch Substitution von Amidgruppen durch Chloratome entstehen außerdem ätherlösliche Amidchloride der Phosphorsäure. Oligomere μ-Imidophosphorsäureamide werden nur in Spuren erhalten. Zur Interpretation der experimentellen Befunde wird die intermediäre Bildung von Phosphorylimidamid, OP(=NH)NH2, und Phosphorylimidchlorid, OP(=NH)CI, angenommen.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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