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1H and 13C NMR analysis of brassinosteroids (1992)

Porzel, Andrea ; Marquardt, Volker ; Adam, Günter ; [et al.]

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 30 (1992), S. 651-657

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ISSN: 0749-1581

Keywords: Brassinosteroids ; 1H and 13C chemical shift assignment ; Partially relaxed ; 1H COSY ; Relayed COSY ; XHCORRD ; HMQC ; HMBC ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The 1H and 13C NMR spectra of the two phytohormones, brassinolide and 24-epi-brassinolide, and the two synthetic analogues 22,23,24-trisepi-brassinolide and (22S,23S)-28-homo-brassinolide, were assigned using 1D and 2D NMR techniques. Independent assignment strategies are presented for the 1H and 13C chemical shifts of the steroidal side-chain.

Additional Material: 5 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260300714

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