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Application of the attached proton test technique in 31P NMR spectroscopy (1984)

Jancke, H. ; Radeglia, R. ; Neels, J. ; [et al.]

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 22 (1984), S. 376-378

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ISSN: 0030-4921

Keywords: Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Intensity modulated 31P NMR spectra were obtained using the pulse sequence published by Patt and Shoolery. This attached proton test (APT) technique for signal assignment could be applied to systems with long-range heteronuclear couplings in P—O—C—H fragments. In a model system derived from the alcoholysis of P4S10 the six reaction products were assigned to the six signals in the 31P NMR spectrum.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1270220606

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