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Liquid chromatographic analysis with electrochemical detection for metoclopramide in human plasma (1987)

Boussairi, A. ; Guyon, F.

Springer

Chromatographia 23 (1987), S. 651-652

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ISSN: 1612-1112

Keywords: Column liquid chromatography ; Metoclopramide ; Electrochemical detection

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Summary A simple, reproducible liquid-chromatographic method for determination of metoclopramide anti-emetic and anti-spasmodic agent is described. Metoclopramide is extracted from alkalinized plasma into diethylether, then separated with a sperisorb CN column and measured through amperometric detection at +1,4 volt vs Ag/ AgCl. The average extraction recovery was 92%. Standard curves were linear and reproducible from 0.05 to 1.5 mg/ L. Within-day CV was better than 6%.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF02311493

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