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Crystal structure of lanthanum(III) oxalate decahydrate (1991)

Huang, Sheng -Hua ; Zhou, Gong -Du ; Mak, Thomas C. W.

Springer

Journal of chemical crystallography 21 (1991), S. 127-131

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ISSN: 1572-8854

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract La2(C2O4)3·10H2O crystallizes in space groupP21/c (No. 14) witha=11.382(6),b=9.624(5),c=10.502(8) Å,β=114.52(4)°, andZ=2. The structure (R=0.029 for 3190 MoKα data) is composed of two-dimensional networks of edge-sharing 1∶5∶3 coordination polyhedra matching the (020) set of planes, each La(III) atom being surrounded by threeη 4 chelating oxalate groups and three aqua ligands with La-O distances in the range 2.518(4)–2.622(4) Å. The remaining water molecules are disordered over seven principal sites in the intervening space.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01161053

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