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Crystal structure of 1,3-(N,N′-benzamide)-2-methyl-1-pentene (1989)

Bocelli, Gabriele

Springer

Journal of chemical crystallography 19 (1989), S. 841-846

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ISSN: 1572-8854

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract Crystals of the title compound are monoclinic (C20H22N2O2): space groupP21/n,a=11.800(3),b=13.820(2),c=11.004(3) Å,β=92.74(3)°. The structure was solved by direct methods and refined by block-matrix least-squares procedure to giveR=0.078 andRw=0.076 for 1960 reflections above 3σ(I). The two amide groups are not coplanar with respect to their benzene rings. An intramolecular N-H⋯O hydrogen bond was found in the molecules which are joined in chains by other strong N-H⋯O hydrogen bonds.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01185350

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