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Crystal and molecular structure of 4-aminoacetyl-N-p-nitrophenylsulfanilamide (1989)

Ghosh, M. ; Basak, A. K. ; Mazumdar, S. K. ; [et al.]

Springer

Journal of chemical crystallography 19 (1989), S. 289-298

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ISSN: 1572-8854

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract The crystal and molecular structure of 4-aminoacetyl-N-p-nitrophenylsulfanilamide (C14H13N3O5S), a derivative of sulfonamide, has been determined from X-ray diffraction data using Cu-Kα radiation. The compound crystallised in the monoclinic space groupP21/c, witha=12.258(9),b=7.339(5),c=16.359(9) Å,β=98.84(4)°. The structure was solved by direct methods and refined by full-matrix least-squares to a finalR value of 0.047 with 2487 unique reflections. In packing, the molecules are found to be stabilised by N-H⋯ O hydrogen bonds.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01194124

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