ISSN:
1573-4803
Source:
Springer Online Journal Archives 1860-2000
Topics:
Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
Notes:
Abstract Titania- and alumina-supported molybdenum-containing systems have been prepared from mechanical mixtures of the support and molybdenum trioxide. The systems have been characterized by X-ray diffraction, temperature-programmed reduction and scanning electron microscopy, and Fourier transform-infrared monitoring of pyridine adsorption has been used to determine surface acidity. Dispersion of the supported phase, and its transformation to well-dispersed species has been attained by mechanical grinding and calcination in air, or by hydrothermal treatment of such mixtures and calcination. In the latter case, a higher dispersion is reached, despite the shorter time of calcination. Also hydrothermally treated samples show a larger concentration of surface Brönsted acid sites.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF00357865
