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Effects of formation of an adduct of trialkylpyrazole with CdBr2 in15N NMR (1998)

Kessenikh, A. V. ; Strelenko, Yu. A.

Springer

Chemistry of heterocyclic compounds 34 (1998), S. 658-662

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ISSN: 1573-8353

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract The15N NMR chemical shifts for the analogous diamagnetic adduct of 3,5-dipropyl-4-ethylpyrazole with cadmium dibromide were measured to obtain reference data for estimating the isotropic paramagnetic NMR shifts of nitrogen in paramagnetic adducts of alkylpyrazoles with transition metal salts. The13C and1H NMR spectra were obtained for the same adduct in conditions of frozen protometallotropic rearrangement of the hydrogen in the NH group and the temperature-dependent NMR spectra of isotopes of Cd were made.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF02252271

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