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Physical properties and structure of silk. III. The glass transition and conformational changes of tussah silk fibroin (1977)

Magoshi, Jun ; Magoshi, Yoshiko ; Nakamura, Shigeo

New York, NY [u.a.] : Wiley-Blackwell

Journal of Applied Polymer Science 21 (1977), S. 2405-2407

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ISSN: 0021-8995

Keywords: Chemistry ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics

Notes: The glass transition, crystallization, and α-β transition of the Tussah silk fibroin were studied by means of DSC (differential scanning calorimetry) and infrared spectroscopy. The endothermic shift due to the glass transition was observed at 162°C. The endothermic peak at 220°C was attributed to the α-β conformational transition from the infrared spectra. The exothermic peak due to the crystallization occurred at 230°C.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/app.1977.070210909

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