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Rate effects in the measurement of polymer transitions by differential scanning calorimetry (1969)

Strella, S. ; Erhardt, P. F.

New York, NY [u.a.] : Wiley-Blackwell

Journal of Applied Polymer Science 13 (1969), S. 1373-1380

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ISSN: 0021-8995

Keywords: Chemistry ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics

Notes: Depending on heating rate, differences as large as 15°C in polymer transition temperatures may be observed in DCS measurements. A heat transfer analysis of the method shows that this rate dependence is a result of a lag in the heat path to the test sample and lag in heat transfer within the sample. Experiments confirmed the analysis. Methods for obtaining the correct values of transition temperatures are given.

Additional Material: 5 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/app.1969.070130704

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