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Free radical polymerization of a sugar residue-carrying styryl monomer with a lipophilic alkoxyamine initiator: synthesis of a well-defined novel glycolipid (1998)

Ohno, Kohji ; Fukuda, Takeshi ; Kitano, Hiromi

Weinheim : Wiley-Blackwell

Macromolecular Chemistry and Physics 199 (1998), S. 2193-2197

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ISSN: 1022-1352

Keywords: Chemistry ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology , Physics

Notes: Controlled free radical polymerization of N-p-vinylbenzyl-2,3,5,6-tetra-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-D-gluconamide (Ac-VLA) was achieved by the nitroxide-mediated free radical polymerization with a lipophilic alkoxyamine “initiator” with a dioctadecyl group in 1,2-dichloroethane at 90°C. The polymerization proceeds in a “living” fashion, providing Ac-VLA polymers with low polydispersity. The hydrolysis of the polymers results in well-defined glycopolymer-carrying amphiphiles, viz., artificial “glycolipids”.

Additional Material: 6 Ill.

Type of Medium: Electronic Resource

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