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Spinmarkierte Oligopeptide als substratanaloge Inhibitoren der Leucinaminopeptidase (1980)

Fittkau, Siegfried ; Damerau, Werner

New York, NY : Wiley-Blackwell

Journal für Praktische Chemie/Chemiker-Zeitung 322 (1980), S. 1032-1038

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ISSN: 0021-8383

Keywords: Chemistry ; Organic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Spin Labeled Oligopeptides as Substrate Analogous Inhibitors of Leucine AminopeptidaseThe synthesis of L-Thr(But)-(L-Phe)n-SL peptides C-terminal labeled with the nitroxide spin label 2,2,5,5-tetramethyl-3-amino-pyrrolidin-1-oxyl, is described and e.s.r. parameters of the labeled compounds are presented. As shown by e.s.r. spectroscopy studies Thr(But)-Phe-SL is a competitive inhibitor of the leucine aminopeptidase and is bound by the enzyme with high affinity.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/prac.19803220621

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