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A Short Syntheses of 1,2-Dimethylazulenes (1992)

Fallahpour, Reza Ali ; Hansen, Hans-Jürgen

New York, NY : Wiley-Blackwell

Helvetica Chimica Acta 75 (1992), S. 2210-2214

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ISSN: 0018-019X

Keywords: Chemistry ; Organic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Dimethyl azulene-1,2-dicarboxylates are reduced with a 4-5 molar excess of DIBAH in Et2O/hexane at 0° to yield the corresponding 2-(hydroxymethyl)-1-methylazulenes which can be further reduced to 1,2-dimethylazulenes on treatment with Et3SiH in TFA at 60° (cf. the Table).

Additional Material: 1 Tab.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/hlca.19920750705

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