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An Alternative Synthesis of [Pd2Cl2(μ-dmpm)2] (1992)

Davies, J. A. ; Dutremez, Sylvain ; Vilmer, M.

New York, NY : Wiley-Blackwell

Journal für Praktische Chemie/Chemiker-Zeitung 334 (1992), S. 34-36

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ISSN: 0941-1216

Keywords: Chemistry ; Organic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: A new, high yield synthesis of [Pd2Cl2(m̈-dmpm)2] (dmpm = bis(dimethylphosphino)methane), which avoids the use of the ill-defined, polymeric substance [PdCl(CO)]n as a starting material, is described. The procedure involves ligand metathesis of [Pd2Cl2(m̈-dppm)2] (dppm = bis(diphenylphosphino) methane) with dmpm using a solvent in which both [Pd2Cl2(m̈-dppm)2] and [Pd2Cl2(m̈-dmpm)2] are only sparingly soluble. Yields of 〉 98% are routinely obtained.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/prac.19923340106

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