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Synthesis of a Novel Annulated C1-Bridged ansa-Metallocene System (1994)

Erker, Gerhard ; Psiorz, Christian ; Krüger, Carl ; [et al.]

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 127 (1994), S. 1551-1553

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ISSN: 0009-2940

Keywords: ansa-Metallocenes ; Fulvenes ; Catalysis, homogeneous ; Ziegler-Natta catalysts ; Chemistry ; Inorganic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: 2,5-Hexanedione (1) was converted into the bis(fulvene) 2, which was then treated with 2 molar equiv. of ethereal meth-yllithium to give the novel annulated C1-bridged dilithium bis(cyclopentadienide) 5. Reagent 5 was treated with MCl4 (M = Ti, Zr) to yield the annulated C1-bridged ansa-metallo-cene dichlorides 6a and 6b, respectively. The homogeneous 6a, 6b/methylalumoxane Ziegler-type systems were employed in propene polymerization reactions.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/cber.19941270834

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