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Conformational studies on B/C-cis- and B/C-trans-morphinan derivatives (1995)

Szabó, Zoltán ; Marton, János ; Hosztafi, Sándor

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 33 (1995), S. 913-916

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ISSN: 0749-1581

Keywords: NMR ; NOE ; selective 2D J spectroscopy ; B/C-cis- and B/C-trans-morphinans ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: An unambiguous structural differentiation of B/C-cis- and B/C-trans-morphinan derivatives (thebainone-A and β-thebainone-A and their 7,8-dihydro derivatives) is provided. The structures were confirmed by NOE difference spectroscopy and selective 2D J-INEPT experiments. In addition, full a priori 1H and 13C NMR assignments of the isomeric pairs studied are presented.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260331114

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