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Sequential proton saturation for the heteronuclear 1D NOE experiment (1992)

Mueller, C. ; Bircher, H. R. ; Bigler, P.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 30 (1992), S. 466-475

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ISSN: 0749-1581

Keywords: Heteronuclear NOE ; Selective pulses ; Shaped pulses ; Sequential excitation ; Improved data accumulation ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: An improved 1D pulse sequence for detecting heteronuclear NOEs on a qualitative level is described and demonstrated. It makes use of shaped selective pulses and takes advantage of sequential perturbation of several proton resonances during one experiment and correspondingly more efficient data accumulation schemes. The method is particularly suitable for assigning quaternary carbons and for establishing connectivities between assigned molecular fragments bound to these quaternary centres.

Additional Material: 7 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260300603

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