ISSN:
0749-1581
Keywords:
Tetramethyllimonene
;
Assignments
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
Dynamic effects of tetramethyllimonene were studied at low temperatures. Nuclear Overhauser effects measured under optimized conditions at 223 K and the results of 2D correlation experiments allowed the identification of two conformers and the assignment of all the proton and carbon resonances. For the determination of exchange and relaxation rates the method of saturation transfer was applied. At temperatures below 223 K further dynamic effects were recognized. Structural information obtained experimentally was compared with the results of Allinger force field calculations.
Additional Material:
8 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260280303