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Mass spectra of trimethylsilyl ethers of some Δ5-3β-hydroxy C 19 steroids (1973)

Brooks, C. J. W. ; Harvey, D. J. ; Middleditch, B. S. ; [et al.]

Chichester : Wiley-Blackwell

Biological Mass Spectrometry 7 (1973), S. 925-948

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ISSN: 0030-493X

Keywords: Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The mass spectra (20 eV electron energy) of a wide range of %Δ5-3β-hydroxy C19 steroid TMS ethers have been examined with the aid of high-resolution mass measurements, together with deuterium and oxygen-18 labelling data. The validity of many previously proposed fragmentation modes has been confirmed. A number of ions regarded as diagnostic have been shown to be less specific than had been formerly supposed. Several novel fragmentations have been observed and investigated.

Additional Material: 13 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/oms.1210070803

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