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Characterization of organic substrates bound to cross-linked polystyrenes by 13C NMR spectroscopy (1982)

Jones, Alan J. ; Leznoff, Clifford C. ; Svirskaya, Polina I.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 18 (1982), S. 236-240

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ISSN: 0030-4921

Keywords: Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The 13C NMR spectra of a wide variety of organic substrates bound to 2% cross-linked polystyrenes may be obtained routinely, provided the resins can be sufficiently swollen. The 13C chemical shifts of polymer-bound trityl alcohol, polymer-bound monotrityl ethers of the symmertrical diols HO (CH2)nOH (n=2, 4, 6, 7, 9 and 10), and some related intermediates in the solid phase synthesis of insect pheromones are presented. 13C shift additivity correlations, differing little from those in free trityl ethers, are drawn.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1270180414

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