ISSN:
1052-9306
Keywords:
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
The use of capillary column gas chromatography mass spectrometry has been investigated for the detection of the presence of estrane-3,17α-diol in horse urine extracts; the detection of this diol confirms the administration of anabolic steroids based upon 19-nortestosterone. To reduce analysis time, but yet maintain a solvent effect in the splitless injection mode, injections have been made at elevated temperatures (190-220°C) using high boiling solvents (dodecane b.p. 214°C and tetradecane b.p. 252°C).
Additional Material:
3 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/bms.1200080808