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Electron crystallography with the EIGER detector (2018)

Tinti, G.Fröjdh, E.van Genderen, E.Gruene, T.Schmitt, B.de Winter, D. A. M.Weckhuysen, B. M.Abrahams, J. P.

International Union of Crystallography (IUCr)

In: IUCrJ

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Publication Date: 2018-02-15

Description: Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a transmission electron microscope. EIGER features a pixel pitch of 75 × 75 µm2, frame rates up to 23 kHz and a dead time between frames as low as 3 µs. Cluster size and modulation transfer functions of the detector at 100, 200 and 300 keV electron energies are reported and the data quality is demonstrated by structure determination of a SAPO-34 zeotype from electron diffraction data.

Keywords: EIGERhybrid pixel detectorselectron crystallographySAPO-34

Electronic ISSN: 2052-2525

Topics: Geosciences , Physics

Published by International Union of Crystallography (IUCr)

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