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  • Volumetrie  (69)
  • Chromatographie, Gas  (67)
  • 42.55  (64)
  • Springer  (200)
  • Periodicals Archive Online (PAO)
  • 1975-1979  (200)
Collection
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  • Springer  (200)
  • Periodicals Archive Online (PAO)
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Year
  • 1
    Electronic Resource
    Electronic Resource
    Excimer ArF/XeF lasers providing high-power stimulated radiation in Ar/Xe and F lines (1977)
    Springer
    Applied physics 14 (1977), S. 231-233 
    Details
    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Lasing in atomic lines of noble gases and fluorine, prior to excimer radiation, was observed in an electric discharge ArF/XeF excimer laser. Some Ar/Xe lines end at metastable levels, which are very important for the formation of ArF/XeF excimer molecules. Five new lasing lines of atomic fluorine have been obtained. Consideration is given to the use of lasing in atomic and molecular lines, that occurs in one burst, in investigations of the excitation kinetics of excimer states under the conditions of a high-pressure electric discharge.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00883096
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  • 2
    Electronic Resource
    Electronic Resource
    Properties and current-voltage characteristics of discharges in waveguide gas lasers (1977)
    Springer
    Applied physics 14 (1977), S. 277-282 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 52
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The paper deals with the properties andI-V characteristics of discharges in narrow capillaries used, for example, for He−Ne waveguide lasers. It has been observed that discharges in He−Ne waveguide lasers are unstable because of the strongly falling characteristic. A theory is presented which assumes that at low currents wall charges restrict the positive column to a narrow plasma channel and are the main reason for the observed falling characteristic. A numerical evaluation for helium gives results which agree well with experimental data.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00882732
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  • 3
    Electronic Resource
    Electronic Resource
    Models of DNA-dye-complexes: Energy transfer and molecular structures as evaluated by laser excitation (1979)
    Springer
    Applied physics 18 (1979), S. 333-338 
    Details
    ISSN: 1432-0630
    Keywords: 87 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Energy transfer in DNA-dye-complexes after excitation in the UV down to 220 nm by means of a tunable laser was investigated. DNA of different base composition and polynucleotides were compared. The dyes proflavine, acridine orange and ethidium bromide were used. The energy transfer from DNA-bases to dye molecules was measured in dependence of the excitation wavelength and the base composition of the DNA. Models of the energy transfer from DNA to dye and of the molecular structures of the DNA-dye-complex (intercalation) could be deduced.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00899685
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  • 4
    Electronic Resource
    Electronic Resource
    Free-electron lasers and masers on curved paths (1979)
    Springer
    Applied physics 19 (1979), S. 47-51 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 42.80
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The possibility of building free-electron lasers and masers with quasi-circular undulators is considered. The two-mirror cavity is replaced by a suitable waveguide. The magnetic field along the orbit has a continuous component superimposed on the alternating one. Besides allowing large freedom for electron guiding and focusing, the structure allows effective negative mass conditions, which may enhance the electron beam modulation when space charge effect are important. Furthermore the radiation frequency can be higher than that in a linear undulator with the same electron energy, and long interaction times are possible in a compact structure.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00900537
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  • 5
    Electronic Resource
    Electronic Resource
    Laser properties of praseodymium pentaphosphate single crystals (1979)
    Springer
    Applied physics 19 (1979), S. 345-351 
    Details
    ISSN: 1432-0630
    Keywords: 78.55 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract PrP5O14, PrxLa1−xP5O14, and PrxY1−xP5O14 (0≦x≦1) single crystals of laser quality were synthesized and their crystallographic and optical parameters measured. Laser emissions in the visible (λ=637.4 nm) with no mirrors in place (superradiance) and also in various optical resonators have been observed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00900479
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  • 6
    Electronic Resource
    Electronic Resource
    Continuous laser oscillation in diatomic molecular sodium (1977)
    Springer
    Applied physics 13 (1977), S. 97-99 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 82.50
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract First cw laser oscillation with thresholds below 1 mW was observed for various B1Пu → X1 ∑ g + transitions of diatomic molecular sodium excited by different argon laser lines in the range of 454–488 nm. For pump powers of 0.5 W output powers up to 3 mW and single-pass gain up to 0.1 cm−1 were obtained. Some properties of the heat pipe laser system are discussed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00890727
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  • 7
    Electronic Resource
    Electronic Resource
    Optically pumped FIR-laser with variable Fabry-Perot output coupler (1977)
    Springer
    Applied physics 13 (1977), S. 383-385 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 42.80
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract An optically pumped FIR laser was operated with a copper mesh Fabr-Perot output coupler. With this device a Gaussian output beam was obtained andthe degree of coupling could be varied continuously, thus allowing optimum coupling. From the measured properties of the wire mesches grains of two FIR laser lines are calculated and the saturation intensities estimated.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00882614
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  • 8
    Electronic Resource
    Electronic Resource
    A magnetic tuning system for dye lasers (1977)
    Springer
    Applied physics 14 (1977), S. 25-28 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 42.80
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A new device for magnetically displacing the output mirror of a laser resonator and synchronously tilting an etalon in order to obtain single-mode tuning of a dye laser over a tuning range of at least 10 GHz is described. Comparatively large displacements with good linearity of a coil mounted on a membrane and placed inside the strong magnetic field of a ring magnet are obtained for currents in the order of several hundred milliamperes. Together with etalon flats of appropriate thickness and reflection mounted in the resonator of the laser a versatile instrument for application in intra and extra cavity spectroscopy has been developed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00882629
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  • 9
    Electronic Resource
    Electronic Resource
    Measurements of some reaction rates of importance in KrF lasers (1977)
    Springer
    Applied physics 14 (1977), S. 393-398 
    Details
    ISSN: 1432-0630
    Keywords: 34 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A flowing afterglow method has been used to study a number of reactions of importance in KrF lasers using NF3 as the fluorine donor. Total rate constants are reported for Kr*(3 P 2)+NF3 and Kr++NF3. The thermal energy attachment coefficient has been measured for NF3 and the cross section for the electron excitation process Kr*(3 P 2) +e→Kr*(3 P 1)+e has been estimated. The relevance of these results to discharge pumped KrF lasers is discussed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00883445
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  • 10
    Electronic Resource
    Electronic Resource
    Argon laser with wall stabilized transverse discharge (1977)
    Springer
    Applied physics 14 (1977), S. 193-197 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 52
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Planar and cylindrical discharges for argon lasers are compared by plasmatheoretical calculations. The maximum laser output power available in the two arrangements is computed in dependence of various parameters neglecting saturation mechanisms. A transverse discharge arrangement confining the positive column by two parallel walls is described and experimental laser threshold values for the current and pressure are reported.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00883089
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  • 11
    Electronic Resource
    Electronic Resource
    Modulation behavior of semiconductor injection lasers (1977)
    Springer
    Applied physics 14 (1977), S. 255-268 
    Details
    ISSN: 1432-0630
    Keywords: 42.80 ; 42.55 ; 85.60
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract GaAs double heterostructure semiconductor injection lasers which now exhibit more than 25000 h cw room temperature lifetime are of great interest for future use as directly modulated transmitters for high bit-rate fiber optical communications. The effects limiting this application are modulation distortions, spectral width and additional spectral broadening in the case of modulation and spontaneous fluctuations of the output power. The dynamic and spectral behavior of injection lasers, the methods of high bit-rate modulation and the improvement of the high bit-rate modulation capability by coupling two lasers are discussed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00882730
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  • 12
    Electronic Resource
    Electronic Resource
    Electron energy loss spectra of dye vapors (1978)
    Springer
    Applied physics 15 (1978), S. 185-190 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Electron energy loss studies of POPOP andp-terphenyl in the vapor phase at an incident electron energy of 25 eV have been performed. The spectra covering an energy loss between 0 and 9 eV revealed a considerable initial triplet population under electron impact excitation. The implications for electron-beam pumped vapor phase dye lasers are discussed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00928206
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  • 13
    Electronic Resource
    Electronic Resource
    High-power argon-ion laser with titanium covered beryllia discharge tube (1978)
    Springer
    Applied physics 15 (1978), S. 229-232 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A new type of discharge tube for high-power argon-ion lasers constructed of a segmented metal-ceramic compound system is described. Up to date, the system has been operating for 1500 h without failure. The maximum cw output is 140 W, limited by the destruction of the mirrors.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00928214
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  • 14
    Electronic Resource
    Electronic Resource
    Ultrashort-pulse generation by lasers with saturable absorbers (1978)
    Springer
    Applied physics 15 (1978), S. 439-450 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 42.65
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A theoretical model for the ultrashort-pulse (USP) generation by lasers with saturable absorbers is presented. The gain medium is assumed to be a two-level system whereas the absorber is described by a four-level system which is characterized by a two-stage absorption process and the pertinent relaxation times. Laser dynamical equations are developed in the rate-equation approximation and boundary conditions appropriate for an unidirectional ring cavity are established. Evolution of USP is investigated for different combinations of parameter values appropriate for solid-state laser systems by computer simulation, employing a finite difference approximation for the dynamical equations. It is shown that USP output is attainable even if the cross-section of the excited-state absorption isgreater than that of the ground-state absorption and the laser is operating just above threshold. In fact, it is found that through the participation of a strong excited-state absorption the discrimination against satellite pulses is enhanced so that single-pulse output is more achievable. Furthermore, it is proposed that single picosecond pulses may be obtainable from relatively broad initial peaks by utilizing the high pulse-selection and pulse-shortening efficiency of the absorber due to the contribution of the excited-state absorption. The applicability of the present model to singlet-triplet crossing and photoisomer formation is also discussed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00886165
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  • 15
    Electronic Resource
    Electronic Resource
    Efficient spectral narrowing and tuning of a cw dye laser with a low-loss diffraction grating (1978)
    Springer
    Applied physics 16 (1978), S. 297-301 
    Details
    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A grating-tuned cw dye laser with an emission bandwidth of less than 1 GHz and output power in excess of 400 mW has been constructed. This was accomplished using a newly developed holographic grating with sinusoidal groove profile, which resulted in an enhanced spectral efficiency up to 94%. The low losses and the broad spectral working range (more than 1000 Å) which can be easily covered by simple rotation make these gratings an attractive single-stage tuning element for low-gain cw lasers.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00885125
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  • 16
    Electronic Resource
    Electronic Resource
    Tunable UV-radiation by stimulated Raman scattering in hydrogen (1978)
    Springer
    Applied physics 16 (1978), S. 151-154 
    Details
    ISSN: 1432-0630
    Keywords: 42.65 ; 42.55 ; 33
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract We observed tunable UV radiation down to 175 nm by SRS of the output of a frequency-doubled dye laser in H2. The high power output of the 4th anti-Stokes to 5th Stokes line generated by the frequency doubled dye laser and the 8th anti-Stokes to 3rd Stokes line generated by the undoubled dye laser represents a broadly tunable coherent radiation source between 189 nm and 2064 nm.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00930379
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  • 17
    Electronic Resource
    Electronic Resource
    A simple and reliable short-pulse dye laser (1977)
    Springer
    Applied physics 13 (1977), S. 109-110 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A simple technique is described that allows the generation of a short pulses (1 ns) from dye lasers pumped by a much longer (7 ns) N2-laser pulse. Dye-laser pulses, either with a narrow bandwidth or a short duration, can thus be obtained with the same N2-laser pump.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00890731
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  • 18
    Electronic Resource
    Electronic Resource
    Quasi-cw laser action in K5Nd(MoO4)4 (1978)
    Springer
    Applied physics 17 (1978), S. 367-370 
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    ISSN: 1432-0630
    Keywords: 42.55 ; 78.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract We report on room temperature quasi-cw laser action in K5Nd(MoO4)4 at a wavelength of 1.067 μm. The crystal was pumped with the 5140 Å line of an argon ion laser. Due to thermal effects actual cw lasing was not possible. Chopping the pump light with a low duty cycle of 1∶1000 leads to quasi-cw laser action and stable output power. We have determined the fundamental laser parameters: threshold pump powerA T=15 mW, slope efficiency η=22%, and internal lossesL=2.5%. In order to explain the measured relaxation oscillations, diffusion of the excited 4f-excitons is considered. According to a recently developed theory, a diffusion constant ofD=2×10−6cm2/s explains the observed results.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00886207
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  • 19
    Electronic Resource
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    Tunable laser via F 2 + and F 2 − colour centers in the spectral region 0.88–1.25 μm (1977)
    Springer
    Applied physics 14 (1977), S. 121-122 
    Details
    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Frequency-tunable generation by means of F 2 + and F 2 − colour centers in a LiF crystal is reported. Colour centers were created by illuminating LiF crystals with electrons of 3 meV energy at the electron current density of 1 μA/cm2. The pumping source was a ruby laser with a peak power of 20 MW, a pulse duration of 20 ns, and a repetition rate of 1 Hz. The frequency tuning is obtained in the range of 0.88–1.25 μm. Discussed are the ways of pumping of colour centers and the possibility of lasing in the spectral region of 0.85 to 2 μm in the type of colour centers under investigation.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00882641
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  • 20
    Electronic Resource
    Electronic Resource
    Polarization spectroscopy with ultrashort light pulses (1979)
    Springer
    Applied physics 18 (1979), S. 257-260 
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    ISSN: 1432-0630
    Keywords: 32 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract We have demonstrated the feasibility of Doppler-free polarization spectroscopy with a train of ultrashort pulses from a synchronously pumped mode-locked dye laser. The sensitivity of the method is compared with saturation spectroscopy with a single-mode laser.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00885511
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  • 21
    Electronic Resource
    Electronic Resource
    High-energy dye laser pumped by wall-ablation lamps (1978)
    Springer
    Applied physics 15 (1978), S. 191-196 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A guideline for the optimum design of linear wall-ablation lamps is presented with a simple empirical formula which describes the luminescent characteristics of lamps. The absolute luminescent efficiency of the wall-ablation lamp was measured. A high-energy dye laser with a quadruple-elliptical cylindrical cavity was constructed using these lamps, and an output energy of 23.3 J (11.6 MW) was obtained with an overall efficiency of 0.31 %. The energy-flow diagram of this laser system was computed with a rate-equation analysis, and the conversion efficiency from electrical input to laser output was determined. One can expect an overall efficiency of about 2 %.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00928207
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  • 22
    Electronic Resource
    Electronic Resource
    Threshold singularities of optically pumped dye lasers (1978)
    Springer
    Applied physics 17 (1978), S. 181-187 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A complete theoretical model for optically pumped dye lasers is studied using the rate equation approach which includes excited singlet and triplet state absorption effects. Closed-form solutions under steady-state conditions reveal a novel nonlinear threshold phenomenon: partial reabsorption of the excited laser light can lead to a discontinuous onset of laser oscillation above laser threshold. Theoretical and experimental results for a transversely and longitudinally pumped rhodamine 6G laser are presented in terms of softmode and hardmode behavior at threshold.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00885253
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  • 23
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    The external-resonator cw spin-flip Raman laser; output characteristics and spectroscopic applications (1979)
    Springer
    Applied physics 19 (1979), S. 205-212 
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    ISSN: 1432-0630
    Keywords: 33 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The characteristics of a stable, external-resonator spin-flip Raman laser (SFRL), pumped by a cw carbon monoxide laser of controlled mode quality and spectral content, are determined using a combination of molecular spectroscopy, Raman amplifier and confocal Fabry-Perot interferometer measurements, and heterodyne detection. Single-frequency output of a free-running external-resonator is demonstrated with an inherent linewidth of 〈10 kHz and a short-term frequency jitter of ≃100 kHz. With the resonator length actively controlled to lock an axial mode frequency to the peak of the spontaneous gain, the linewidth of the SFRL output was maintained below 2 MHz. In this mode of operation, small variations in the output tuning rate, corresponding to the magnetic field dependence of the conduction-electrong-factor, were calibrated. Molecular absorption spectra obtained using gas cells both inside and outside the resonator have been used to illustrate the high resolution, wide-range tuning capability and sensitivity of the system. Lambda-doubling of the $$^2 \pi _{3/2} $$ of the Q-branch head of nitric oxide was measured for values ofJ down to 13/2, below which the splitting is less than the Doppler width. The splittings agreed with predictions using parameters obtained by conventional spectra for higherJ-values.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00932399
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  • 24
    Electronic Resource
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    New FIR laser lines from optically pumped methanol analogues (1979)
    Springer
    Applied physics 19 (1979), S. 241-242 
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    ISSN: 1432-0630
    Keywords: 33 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Several new laser lines using optically pumped deuterated methanol molecules have been discovered. These not only increase the spectral coverage of pumped methanol isotopes but may assist in the assignment of a molecular structure.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00932405
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  • 25
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    Efficient single-mode operation of a standing-wave dye laser (1979)
    Springer
    Applied physics 19 (1979), S. 399-403 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The selection of a single longitudinal mode of a dye laser can be achieved with double or triple Michelson reflectors instead of Fabry-Perot etalons inside the laser cavity. These systems can be adapted to commercial multimode dye lasers. They provide a high efficiency and a good geometrical quality of the output beam. With a 7 watt pump power (λ=514.5 nm line of the Ar+ laser), a tunable output power of 1 watt was obtained at the peak of R6G, in the main output beam; the total single-mode power, including the auxiliary output beams, exceeded 1.4 watt. These results correspond to efficiencies of 14% and 20%, respectively (24% and 30% slope efficiencies). We discuss in the text why these efficiencies are comparable to those of ring lasers. In the infrared, with a 4.5 watt pump power (red lines of a Kr+ laser), 250 mW of single-mode output power in the main output beam was obtained at 780 nm with Oxazine 750.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00930103
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  • 26
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    Spectral coincidences between CO-Laser and nitric-oxide. A reinvestigation (1979)
    Springer
    Applied physics 19 (1979), S. 427-429 
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    ISSN: 1432-0630
    Keywords: 33 ; 35 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Spectral coincidences between CO-laser lines and NO fundamental absorption lines were reinvestigated in order to resolve discrepancies between recently published papers. The absorption of CO laser radiation by NO and NO/Ar mixtures was measured and fitted by calculations using a Voigt profile for the NO line shapes. A new coincidence with a frequency offset of less than the NO Doppler width was found.
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    URL: http://dx.doi.org/10.1007/BF00930107
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  • 27
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    Extended spectral distribution of lasing transitions in a liquid-nitrogen cooled CO-laser (1979)
    Springer
    Applied physics 19 (1979), S. 439-440 
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    ISSN: 1432-0630
    Keywords: 07 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A liquid-nitrogen cooled12C16O laser was operated both Q-switched and cw. A total of 276 lasing transitions were observed in cw using an intracavity grating for line selection. In the Q-switch mode, 230 lines occurred without dispersive element in the cavity.
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    A broadly tunable IR waveguide Raman laser pumped by a dye laser (1979)
    Springer
    Applied physics 18 (1979), S. 235-241 
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    ISSN: 1432-0630
    Keywords: 42.65C ; 42.55 ; 33.20
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Design and performance characteristics of a tunable ir waveguide Raman laser pumped by a high power dye laser are described. Using SRS up to third Stokes order in compressed H2, the wavelength range from 0.7 to 7 μm has been covered without gaps. Taking advantage of a waveguide structure in the scattering chamber, energy conversion efficiencies better than 1% with power levels in excess of 80 kW for the third Stokes component have been achieved. The experimental results support the theoretical predictions that a 4-wave parametric process is responsible for the production of the third Stokes component.
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    URL: http://dx.doi.org/10.1007/BF00885508
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    A free-electron laser in a uniform magnetic field (1979)
    Springer
    Applied physics 20 (1979), S. 41-50 
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    ISSN: 1432-0630
    Keywords: 41 ; 42.55 ; 95
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The interaction of free electrons and free electromagnetic radiation, in the presence of a uniform magnetic field, can result in stimulated emission or absorption. We analyze the dynamics of single electrons by solving the classical, relativistic Lorentz force equations of motion in these combined fields. An electron may gain energy from, or lose energy to, the radiation field, depending crucially on the phase and oscillation frequency of the electron's helical motion within the superposed, circularly polarized light wave. To first order in the radiation field strength, electrons in a monoenergetic, uniformly distributed beam become spatially bunched, but there is no net energy change. To second order, however, the beam may experience a gain or loss of energy, corresponding to attenuation or amplification of radiation. We compare the bunching of this laser process to the bunching processes involved in 1) the Stanford free-electron laser and 2) the cyclotron maser, and find significant differences in each case. Our analytic results provide a clear, simple picture of the interaction process, and can be useful in exploring light amplification in astrophysical magnetic fields, the magnetosphere, or in laboratory devices.
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    A laser accelerator (1979)
    Springer
    Applied physics 20 (1979), S. 61-65 
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    ISSN: 1432-0630
    Keywords: 42.55
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract We show that a laser can efficiently accelerate charged particles if a magnetic field is introduced to improve the coupling between the particle and the wave. Solving the relativistic equations of motion for an electron in a uniform magnetic field and superposed, circularly polarized electromagnetic wave, we find that in energy-position phase space an electron traces out a curtate cycloid: it alternately gains and loses energy. If, however, the parameters are chosen so that the electron's oscillations in the two fields are resonant, it will continually accelerate or decelerate depending on its initial position within a wavelength of light. A laboratory accelerator operating under these resonant conditions appears attractive: in a magnetic field of 105 Gauss, and the fields of a 5×1012 W, 10 μm wavelength laser, an optimally positioned electron would accelerate to 700 MeV in only 10m.
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    A double-wavelength nitrogen-laser-pumped dye laser (1979)
    Springer
    Applied physics 20 (1979), S. 97-99 
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    ISSN: 1432-0630
    Keywords: 42.55
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A narrow-band tunable double-wavelength dye laser with a bandwidth of 0.1 cm−1 is described. The output at one of the wavelengths is found to be completely linearly polarized in the plane of incidence.
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    URL: http://dx.doi.org/10.1007/BF00901793
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    Excimer gas-discharge tunable ArF laser (1977)
    Springer
    Applied physics 13 (1977), S. 107-108 
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    ISSN: 1432-0630
    Keywords: 42.55
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Intense laser oscillation has been observed from ArF molecules at 1933 Å. Excitation of the gas mixture NF3:Ar:He=1:55:630 at total pressures above 2.1 atm was produced by a transverse electric discharge. The range of fine tuning was from 1927 Å to 1936 Å. An output energy of 0.8 mJ was measured from a laser pulse 15 ns in duration.
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    Polarization properties of a single-mode gas laser in transverse magnetic fields (1978)
    Springer
    Applied physics 17 (1978), S. 257-267 
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    ISSN: 1432-0630
    Keywords: 42.55 ; 32.60
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The effect of transversally applied magnetic fields on the polarization behavior of a single-mode gas laser is theoretically investigated, stressing the importance of the additivity of respective contributions influencing the time evolution of polarization parameters. By adding a new element to the existing theory, namely the contribution of magnetic-field-free regions in the active medium, and by considering the relatively large effects that small cavity anisotropies can cause, several apparent discrepancies between experiments and existing theory are resolved.
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    Feedback controlled self-excitation of optical pulses in a CW dye ring laser (1978)
    Springer
    Applied physics 15 (1978), S. 59-63 
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    ISSN: 1432-0630
    Keywords: 42.55
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    Notes: Abstract Feedback controlled self-excitation of optical pulses of nanosecond duration has been observed to occur rather reliably in a CW dye ring laser, oscillating in a traveling mode. These observations are described analytically by means of a direct time domain approach. It is shown that a steady-state Gaussian pulse whose time duration determined from the self consistency condition in terms of system characteristics describes accurately the observed pulse behaviors.
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    Intrapulse thermally induced wavelength shift in a distributed feedback dye laser (1979)
    Springer
    Applied physics 19 (1979), S. 39-41 
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    Keywords: 42.55 ; 42.65
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    Notes: Abstract It is shown that when a distributed feedback dye laser is used to generate a train of picosecond pulses, the narrow lines observed in the spectrum are not longitudinal modes, but are due to the intrapulse refractive index changes caused by the heating effect of the pumping pulse.
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    Laser-fluctuation measurements in a bath of strong Gaussian noise (1979)
    Springer
    Applied physics 18 (1979), S. 415-419 
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    Keywords: 42.55
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Remarkable intensity fluctuations were observed in the LiNdP4O12 (LNP) laser by placing a moving ground-glass plate across the ouput beam. Resonance-like behaviors were also observed by tuning the moving velocity of the ground-glass plate, with respect to relaxation oscillations. Classical rate equations including the modulation term were given to explain the observed phenomena. Similar intensity fluctuations corresponding to relaxation oscillations were observed when the LNP laser light beam was coupled to an optical fiber.
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    Efficient dye lasers pumped by a XeCl excimer laser (1979)
    Springer
    Applied physics 19 (1979), S. 35-37 
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    Keywords: 42.55
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Results of an investigation of 19 organic dyes pumped by a 1.7 MW discharge-pumped XeCl excimer laser are reported. The dye-laser emission covered a wide wavelength range from 340 nm to 710 nm.P-terphenyl shows efficient laser action. The highest energy conversion efficiency exceeds 40% in visible region. In comparison with 250 kW nitrogen laser pumping, higher efficiencies are obtained for most of these dyes in the same dye-laser configuration.
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    On the interaction of stimulated spin-flip raman scattering and stimulated recombination radiation in InSb (1979)
    Springer
    Applied physics 19 (1979), S. 185-189 
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    Notes: Abstract We have studied the interaction of stimulated spin-flip Raman scattering and stimulated recombination radiation in n-InSb using a CW CO pump laser. A change in linewidth and output power of second Stokes spin-flip radiation is observed when the tuning curve of the first Stokes stimulated spin-flip radiation and the stimulated recombination radiation cross. The observations are explained using a simple rate equation model.
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    NdP5O14 and NdAl3(BO3)4 lasers at 1.3 μm (1979)
    Springer
    Applied physics 18 (1979), S. 77-80 
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    Keywords: 42.55 ; 78.55
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    Notes: Abstract We report, for the first time, on room temperature cw laser action of NdP5O14 and NdAl3(BO3)4 at 1.3 μm wavelength. The emission cross sections of the transition4 F 3/2→4 I 13/2 are 0.24·10−19 cm2 and 1.74·10−19 cm2, respectively. The lowest observed threshold was 45 mW and the slope efficiency was nearly 10%. The minimum threshold is expected to be about 5 mW of absorbed pump light for both materials.
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    Collisional effects upon optical coherences: Experimental study in a xenon three-level system (1979)
    Springer
    Applied physics 20 (1979), S. 83-88 
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    ISSN: 1432-0630
    Keywords: 32 ; 34 ; 42.55
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    Notes: Abstract Laser induced nonlinear absorption profiles in a three-level system have been recorded to study the effect of elastic collisions upon optical coherences. In our particular system, the signal is due to a pure double-quantum term, where we have separated the effect of phase-interrupting collisions from the effect of velocity-changing collisions. Experimental results show that the effect of velocity-changing collisions is very small, and that broadening of the signal is due to phase-interrupting collisions mainly. We are able to determine the increase of the decay rate of the coherent superposition (the “coherence”) of two levels of same parity [Dγ 13/dp=(6.5±1) MHz/Torr] and an upper limit for the mean velocity change (ũ≲5m/s).
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    Dye lasers and intermolecular and intramolecular energy transfer processes (1979)
    Springer
    Applied physics 19 (1979), S. 165-170 
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    Keywords: 33 ; 42.55
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    Notes: Abstract Computer calculations of ETDL performance indicate that dye laser output can be manipulated by an appropriate choice of a donor (absorber)-acceptor (dye) couple. Studies of relevant laser induced inter- and intramolecular energy transfer processes are presented.
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  • 42
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    Small-scale instability of a pulse front traversing a resonant saturable absorber (1979)
    Springer
    Applied physics 19 (1979), S. 221-224 
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    ISSN: 1432-0630
    Keywords: 42.10 ; 42.55 ; 42.65
    Source: Springer Online Journal Archives 1860-2000
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    Notes: Abstract Wave front of a light pulse is shown to be unstable as it propagates through a resonant saturable absorber, if its frequency is higher than the resonance frequency of the absorber. When ΔωT 2∼1, a small-scale transverse instability with the dimension of (λl abs)1/2 grows rapidly. Its growth-rate is of the order of the small-signal-absorption length of the medium.
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    A simple transition-locked and polarization-forced multi-line oscillator for high-power CO2-laser systems (1979)
    Springer
    Applied physics 19 (1979), S. 257-264 
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    Keywords: 42.55
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Employing injection-locking techniques an oscillator configuration was found comprising in a simple way all the features required for fusion directed high-power CO2 laser systems. The oscillator provides emission in single axial modes on rotational transitions which can be freely selected by feeding fluencies of a few mW/cm2 at the particular transition into the oscillator cavity. In the same way simultaneous emission on selectable lines can be achieved. By the same principle the oscillator can be forced to emit in any orientation of polarization. The set up is relatively simple, the alignment rather uncritical, and the operation reliable. Gaussian-shaped nanosecond pulses with low forepulse power are produced with the help of a pulse cutter and saturable multiline absorber. The set up is described and its features are demonstrated by measurements.
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    Reaction kinetics of excimer lasers using NF3 (1977)
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    Applied physics 13 (1977), S. 1-3 
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    Notes: Abstract Disappearance of NF3 and appearance of NF2 and N2F2 in an excimer laser is followed quantitatively with a mass spectrometer. A model for the kinetics is presented.
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    Performance of NdLa pentaphosphate laser pumped by nanosecond pulses (1977)
    Springer
    Applied physics 13 (1977), S. 55-58 
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    Keywords: 42.55 ; 78.60
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    Notes: Abstract NdxLa1−xP5O14 (0.25≦x≦1) single crystals, placed within a confocal optical resonator, were pumped with ruby laser fundamental and second-harmonic nanosecond pulses. In both cases laser oscillations at 1.05 μm exceeding in duration many times the pumping pulse were obtained.
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    Nonlinear absorption spectroscopy of the ethane molecule (1977)
    Springer
    Applied physics 14 (1977), S. 343-350 
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    Keywords: 33 ; 42.55
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    Notes: Abstract By means of nonlinear absorption spectroscopy data necessary for the interpretation of molecular spectra can be obtained in such spectral regions, where conventional spectroscopic methods yield only a quasi-continuous absorption curve. Using a Zeeman-tuned He−Ne laser at the wavelength of 3.39μm we have measured significant differences in the intensity and temperature behaviour for several ethane absorption lines, the analysis of which made possible a preliminary qualitative assignment of these lines.
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    A high-power single-mode cw dye ring laser (1977)
    Springer
    Applied physics 14 (1977), S. 377-380 
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    Keywords: 42.55 ; 42.65
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    Notes: Abstract Due to spatial hole burning, standing-wave dye lasers require a large amount of selectivity inside the cavity for single-mode operation. The output power of these lasers is limited by losses caused by the frequency selecting elements. In a travelling-wave laser, on the other hand, spatial hole burning does not exist, thereby eliminating the need for high selectivity. A travelling-wave cw dye laser was realized by unidirectional operation of a ring laser, yielding single mode output powers of 1.2 W at 595 nm and of 55 mW in the UV-region with intracavity frequency doubling.
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    Instability of laser cw oscillation in the presence of a passive medium (1978)
    Springer
    Applied physics 15 (1978), S. 265-270 
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    Notes: Abstract For a homogeneously broadened two-level ring laser model the stability of the cw laser oscillation in the presence of a passive medium is investigated. The passive material is treated similar to the active material, but without an external pumping mechanism. Stable and unstable regions are shown for various parameters. The stability region of the cw solution becomes extremly small for certain parameters.
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    Dynamic mode interaction in multi-mode laser diodes (1978)
    Springer
    Applied physics 16 (1978), S. 155-158 
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    Keywords: 42.55 ; 78.60 ; 85.60
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    Notes: Abstract Dynamic characteristics of laser diodes are numerically calculated on multi-mode rate equations, including spatial relaxing interaction causing mode competitions or jumps. It is revealed that the interaction effect is classified into three cases [“independent (or inhomogeneous)”, “competition (or intermediate)”, and “monopoly (or ideally homogeneous)”], that an optimum relaxing coefficient value exists to minimize relaxation oscillations in rise and decay transients, and that the optimum value is related to the relaxation period. Calculated results are discussed in comparison with the experimental results.
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    Cw oscillation at 1.05 and 1.32 μm of LiNd(PO3)4 lasers in external resonator and in resonator with directly applied mirrors (1979)
    Springer
    Applied physics 20 (1979), S. 329-334 
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    Keywords: 42.55
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    Notes: Abstract The room temperature cw oscillation at 1.05 and 1.32 μm of lithium neodymium tetraphosphate [LiNd(PO3)4, LNP] lasers in an external resonator and, for the first time, also in a Fabry-Perot resonator with directly applied mirrors is reported. The growth and fluorescence properties of the LNP crystals are briefly described. Laser parameters such as threshold pump power, output power, differential efficiency, optical gain, emission cross section and laser modes are both measured and calculated. Laser experiments show the threshold pump power to be lower for 1.05 μm than for 1.32 μm emission because of the smaller emission cross section; the pump power density is lower for the external resonator than for the Fabry-Perot resonator because of its higher mode losses.
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    Effect of laser dye deterioration on performance (1977)
    Springer
    Applied physics 14 (1977), S. 199-203 
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    Keywords: 42.55 ; 82.50
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    Notes: Abstract Loss of gain in a dye medium as a result of decomposition by pump photons is considered in terms of disappearance of dye molecules and the appearance of a new, single chemical product having absorption in the fluorescence band. The cases of small signal gain and saturated gain are applied to a single pass through a transversely excited amplifier. Loss of output, defined as “quantum yield of laser deterioration”,Q L , is related to the true quantum yield of molecular destruction of the dye,Q M , and other known parameters. For the experimentally common, saturated gain condition, the smallestQ L can be isQ M , which requires a photochemically bleachable dye with high gain, preferably at high concentration, in a long cavity, operating at high injection and pumping fluxes. Reversing these conditions, the highest valueQ L can be, compared withQ M , is unrestricted.
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    Measurement of the diameter of a laser beam (1978)
    Springer
    Applied physics 17 (1978), S. 303-307 
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    Notes: Abstract A new and simple technique for measuring the effective diameter of a laser beam used in material processing is described. The time for the temperature of a spot heated by the laser beam to rise to 90% of equilibrium is compared with that predicted theoretically for a Gaussian TEM00 laser beam. A Gaussian beam diameter equivalent is thus deduced. This calculated diameter is of particular relevance to applications where the laser is used as a heat source.
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    Nonstationary intracavity stimulated raman scattering by polaritons (1978)
    Springer
    Applied physics 17 (1978), S. 393-400 
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    Keywords: 42.55 ; 42.65
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    Notes: Abstract Stimulated Raman scattering by polaritons when employing a nonlinear crystal inside the cavity of the laser with Q-switching and locked to fundamental frequency was theoretically studied. The equations were formulated describing the dynamics of the fundamental, Stokes and polariton waves under the assumption of instant Q-switching and uniformity of radiation except in the longitudinal direction. Numerical solutions of the equations were found and analysed. We demonstrate the influence, on generation characteristics, of the most important parameters, such as the effective nonlinearity, the initial level of population inversion, the feedback of the Stokes wave and the group mismatch between a Stokes and a pump wave. Optimum generation conditions are determined. Possibilities of the method are discussed for the generation of a) giant pulses which are controllable with regard to carrier frequency and duration but are unachievable with other methods, b) Stokes pulses of very small duration and high energy having sharp trailing edges, and c) analogous polariton pulses in the middle and far infrared range. The generation using a number of polariton branches in LiNbO3 was considered as an example. Calculations are in qualitative agreement with experimental data.
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    High-power tunable IR Raman lasers (1978)
    Springer
    Applied physics 17 (1978), S. 211-232 
    Details
    ISSN: 1432-0630
    Keywords: 42.55 ; 42.65 ; 42.80
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Physical principles, new ways and means of creation, schemes, characteristics and features of efficient high-power tunable pulse Raman lasers, operating in the near and middle ir are reviewed. The paper includes: tunable dye and Nd lasers as pump sources; promising active media and their optimal excitation methods; optical systems for producing spatially homogeneous pumping; the physics of Raman oscillators and their practical schemes, efficient high pulse energy liquid N2 and compressed H2 Raman oscillators, covering several bands in the range between 1.4 and 9.2 μm; the physics and construction of efficient tunable Raman amplifiers-convertors, amplifying in the saturation regime of spontaneously scattered or beforehand produced and collimated external Stokes signals, obtained in the spectral range between 0.83 μm and 18 μm. Raman laser using a, so-called, broadband pump where the linewidth of pumping light is broader than the spontaneous scattering linewidth, are also discussed. Features of both amplification and oscillation regimes of such broadband pumped Raman lasers are reported, and conditions for the efficient frequency conversion are determined.
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    URL: http://dx.doi.org/10.1007/BF00886950
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    Multiwatt optically pumped ammonia laser operation in the 12–13 μm (1978)
    Springer
    Applied physics 17 (1978), S. 317-320 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Design and operating caracteristics of high pulse repetition rate NH3 laser producing up to 20 W of average output power are described. The NH3 laser, operating in the 12–13 μm region was optically pumped with a high pulse repetition rate TEA CO2 laser. Dependences of the NH3 laser output on the pump energy, ammonia and buffer gas pressures and pulse repetition rate have been studied. The conversion efficiency of up to 16% has been received.
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    URL: http://dx.doi.org/10.1007/BF00886961
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    Measurement of the transition strength of the 00o2 9.4 μm sequence band in CO2 using a tunable diode laser (1978)
    Springer
    Applied physics 17 (1978), S. 349-353 
    Details
    ISSN: 1432-0630
    Keywords: 35 ; 42.55 ; 42.68
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract We report the first accurate measurements of the transition strengths and linewidths of the 00o2 9.4 μm sequence lines of CO2. This sequence band is found to be very similar to the regular 00o1 laser band, except for an experimentally determined factor of 1.89±0.12 increase in transition strength (if the CO2 molecule is treated as a simple harmonic oscillator the theoretical increase in transition strength is 2.0). The laser absorption spectrometer used for these measurements can detect absorption coefficients in CO2 of ≈10−7 m−1, and we discuss the feasibility of using this sensitivity to monitor rare isotopic forms of CO2.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00886204
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    Tunable simultaneous double-wavelength operation of a cw CO2 laser (1979)
    Springer
    Applied physics 19 (1979), S. 243-245 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Stable step-tunable simultaneous double-wavelength emission from any branch combination of the 9.6 and 10.6 μm bands of a cw CO2 laser is reported in which the relative strengths of the two signals may be controlled.
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    URL: http://dx.doi.org/10.1007/BF00932406
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    Tunable coherent radiation source covering a spectral range from 185 to 880 nm (1979)
    Springer
    Applied physics 18 (1979), S. 177-181 
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    ISSN: 1432-0630
    Keywords: 42.55 ; 42.65 ; 33
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract We have studied experimentally stimulated Raman scattering and 4-wave-interaction processes occuring in hydrogen gas, which is excited by a Nd:YAG-pumped dye laser. The tuning ranges of the various Stokes and anti-Stokes lines, which are generated with high efficiency, cover the spectrum from 185 to 880 nm without a gap.
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    URL: http://dx.doi.org/10.1007/BF00934413
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    Influence of collisional coupling on the energy extraction from theB, C, andD state in KrF (1979)
    Springer
    Applied physics 20 (1979), S. 129-134 
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    ISSN: 1432-0630
    Keywords: 42.55 ; 33 ; 82.50
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Collisional coupling between theB, C, andD states of KrF is measured in a discharge pumped KrF laser. Detection of the time resolved populations in the three states via measurement of the side fluorescence in theB→X, C→A, andD→X bands is used to record the collisional relaxation from theC andD state to theB state during laser emission. The experimentally determined limits for the collisional coupling times are τB-C≦1 ns and τB-D,τC-D〈20 ns at total pressures of 2 bar. Investigation of theB→X fluorescence band shows that the vibrational manifold of theB state is not thermalized during laser emission. TheV-V,T coupling time is estimated to be τV-V,T=4±2 ns. The influence of collisional coupling on energy extraction in the KrF laser is discussed.
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    URL: http://dx.doi.org/10.1007/BF00885933
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    Influence of the inversion depletion in the active medium on the evolution of ultrashort pulses in passively mode-locked solid-state lasers (1979)
    Springer
    Applied physics 20 (1979), S. 237-245 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract An analytical treatment of the ultrashort-pulse generation in a solid-state laser is given taking into account gain saturation. The probability for the breakdown of the picosecond-pulse evolution caused by the amplification depletion is calculated. The influence of the active medium saturation on the satellite-pulse probability is investigated. Both probabilities characterize the mode-locking behaviour of the laser system and are calculated for various laser parameters to find an optimum laser regime.
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    URL: http://dx.doi.org/10.1007/BF00886024
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    Coherent γ-emission by stimulated annihilation of electron-positron pairs (1979)
    Springer
    Applied physics 19 (1979), S. 127-130 
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    ISSN: 1432-0630
    Keywords: 42.55 ; 42.65
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The possibility of using stimulated emission from the recombination of electron-positron pairs for obtaining coherent γ-rays is considered. The critical number of pairs needed for the process is calculated.
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    URL: http://dx.doi.org/10.1007/BF00900548
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    CW HCN laser gain in a hollow dielectric rectangular cross-section discharge tube (1979)
    Springer
    Applied physics 19 (1979), S. 359-361 
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    ISSN: 1432-0630
    Keywords: 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract This paper describes a 1 m-long CW HCN discharge laser with a hollow dielectric rectangular discharge tube of 5×20 cm2 cross-section. For optimum working conditions, the characteristics of the amplifying medium have been made constant over the cross-section, by using an additional magnetic field. Then, the unsaturated gain for the 337 μm line is 6.8% m−1. It is shown to be dependent on the smaller dimension of the cross-section rather than on the other dimension. By using the tube as a waveguide, laser output power of 1 Watt might be obtained with a discharge length of 4 m, instead of the 12m-long discharge required to get the same output power from a cylindrical waveguide laser.
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    URL: http://dx.doi.org/10.1007/BF00900481
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    Selective laser excitation of bases in nucleic acids (1979)
    Springer
    Applied physics 20 (1979), S. 257-259 
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    ISSN: 1432-0630
    Keywords: 87 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Selective electronic excitation of single kinds of DNA bases were performed with dye lasers. Different DNA-dye-complexes were used and the selective excitation could be proved by the varying strength of the interaction between the bases and the dye molecules.
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    URL: http://dx.doi.org/10.1007/BF00886028
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    Powerful laser systems with phase conjugation by SMBS mirror (1979)
    Springer
    Applied physics 20 (1979), S. 261-264 
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    ISSN: 1432-0630
    Keywords: 42.65 ; 42.55
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The method of Stimulated Mandelshtam-Brillouin Scattering (SMBS) is utilized in a powerful laser to obtain better transverse beam quality by phase conjugation. The principle is explained, and the conclusions are substantiated by experimental results.
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    URL: http://dx.doi.org/10.1007/BF00886029
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    Packed high-performance GC-columns (about 50000 HETP) for profile analysis of carcinogenic polycyclic aromatic hydrocarbons in foods, mineral oil products, vehicle exhaust- and cigarette smoke condensate etc. (1976)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 279 (1976), S. 139-140 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von Polycyclen in Lebensmitteln, Erdölprodukten, Abgasen, Tabakrauch ; Chromatographie, Gas ; gepackte Glassäulen
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
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    URL: http://dx.doi.org/10.1007/BF00440807
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    Anwendung der Radio-Gas-Chromatographie bei der Identifizierung von Hormonmetaboliten im Gewebe (1976)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 279 (1976), S. 161-162 
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    ISSN: 1618-2650
    Keywords: Nachw. von Hormonmetaboliten in Biolog. Gewebe ; Chromatographie, Gas ; Radio-GC
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
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    URL: http://dx.doi.org/10.1007/BF00440828
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    Diphenyl thiovioluric acid: A new extractive indicator for iron(II) (1976)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 279 (1976), S. 206-206 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Eisen(II) mit Diphenylthioviolursäure als Indicator ; Volumetrie ; EDTA
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
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    URL: http://dx.doi.org/10.1007/BF00424113
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    Beiträge zur titrimetrischen Bestimmung von dimeren Hydroxyaldehyden (1975)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 276 (1975), S. 201-204 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Glykolaldehyd, Glycerinaldehyd, Hydroxyaldehyden ; Volumetrie ; Dimere
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Es wurden die Möglichkeiten für die titrimetrische Bestimmung von dimerem Glykolaldehyd (Fp: 94–96° C) und dl-Glycerinaldehyd (Fp: 138–141° C) untersucht. Die systematischen Fehler der auf Grund verschiedener funktioneller Gruppen durchführbaren Messungen sind von der Stabilität ihrer cyclischen Halbacetale sowie von den ihrer Depolymerisation folgenden weiteren Gleichgewichten bestimmt. Das aus dem dl-Glycerinaldehyd gebildete Halbacetal besitzt höhere Stabilität als dasjenige aus dem Glykolaldehyd. Mit der Hydrogensulfit-Methode werden 95–96%, mit der Hydroxylamin-Methode dagegen 98–99% vom wahren Wert gefunden. In Wasser gelöst zersetzt sich der Glykolaldehyd verhältnismäßig rasch, und das Gleichgewicht kann durch beide Aldehydreaktionen quantitativ gegen die Monomerenform verschoben werden. Unsere Untersuchungen ergaben, daß die Hydroxylamin-Methode zur Bestimmung der in Form cyclischer Halbacetale kristallisierenden, dimeren Hydroxyaldehyde Vorteile gegenüber der Hydrogensulfit-Methode bietet.
    Notes: Abstract Possibilities for the titrimetric determination of dimeric glycolaldehyde (m.p. 94–96° C) and dl-glyceraldehyde (m.p. 138–141° C) have been investigated. The systematic errors based on different functional groups depend on the stability of the cyclic semiacetals and on the subsequent equilibria established after their depolimerisation. The semiacetal of dl-glyceraldehyde is more stable than that of glycolaldehyde. 95–96% and 98–99% of the real content were found by the hydrogensulphite and hydroxylamine methods, respectively. Glycolaldehyde decomposes rather quickly in aqueous solution and the equilibrium can be shifted towards the monomeric form by both the aldehyde reactions. The hydroxylamine method proved to be more advantageous for the determination of the dimeric hydroxyaldehydes, which cristallise in the form of cyclic semiacetals.
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    Gas-chromatographische Bestimmung von Mono-, Di- und Triäthylenglykol in Wasser (1976)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 280 (1976), S. 32-32 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Äthylenglykol, Diäthylenglykol, Triäthylenglykol in Wasser ; Chromatographie, Gas
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00443548
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    Titrimetric determination of mercaptans with trivalent cobalt (1976)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 278 (1976), S. 128-128 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Mercaptanen mit Kobalt(III) ; Volumetrie
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
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    URL: http://dx.doi.org/10.1007/BF00432575
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    Assay of mixtures of hydrazine and other nitrogen bases by thermometric titrimetry (1976)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 280 (1976), S. 373-376 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Hydrazin, Ammoniak, Anilin, Hydroxylamin, Thiocyanat, Dimethylhydrazin im Gemisch ; Volumetrie ; thermometrisch
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Summary Binary mixtures of hydrazine and one of the following N-containing bases: ammonia, aniline, hydroxylamine, thiocyanate and unsymmetrical dimethyl hydrazine have been assayed thermometrically. The titrations are based both on the basic and the reducing properties of the compounds. For example, whilst for mixtures of hydrazine and ammonia, the total base content is determined by an acid/base titration, and the hydrazine component is determined by oxidation with bromate ion; for mixtures containing aniline or hydroxylamine, serial titration with bromate ensures that all the hydrazine is oxidised before the onset of oxidation of the other component. Mixtures of hydrazine and UDMH have been assayed in both aqueous and non-aqueous media and a comparison of results has been reported. The main advantage of the proposed methods is that they can be applied to industrial samples, which would render other methods impossible.
    Notes: Zusammenfassung Binäre Mischungen von Hydrazin mit Ammoniak, Anilin, Hydroxylamin, Thiocyanat und asymmetrischem Dimethylhydrazin wurden thermometrisch analysiert. Sowohl die basischen als auch die reduzierenden Eigenschaften des Hydrazins bilden die Grundlage der Titrationen. Zum Beispiel wird im Gemisch Hydrazin/Ammoniak der Gesamtbasengehalt acidimetrisch ermittelt und die Hydrazinkomponente durch Oxydation mit Bromat bestimmt. Im Gemisch Anilin/Hydrazin oder Hydroxylamin/Hydrazin wird mit Bromat zunächst alles Hydrazin oxydiert, bevor die Oxydation der zweiten Komponente einsetzt. Mischungen von Hydrazin mit asym. Dimethylhydrazin werden in wäßrigem und auch in nichtwäßrigem Medium ausgeführt und die Ergebnisse verglichen. Der Hauptvorteil der beschriebenen Verfahren besteht darin, daß auch industrielle Proben untersucht werden können, bei denen andere Verfahren versagen würden.
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    URL: http://dx.doi.org/10.1007/BF00439074
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    Titrimetric determinations of cryptands and cryptates (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 298 (1979), S. 358-362 
    Details
    ISSN: 1618-2650
    Keywords: Best von Kryptanden, Kryptaten ; Volumetrie ; HCl, Metall-Standardlösung, Standardzugabeverfahren
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Summary Using bromocresol green as a visual endpoint indicator solutions of the cryptands [2.2.1] and [2.2.2] can be determined by titration with HCl in the concentration range of 10−1–10−3 M with relative standard deviations of 0.2–0.4 %. If both cryptand and cryptate are present in one solution, then the sum of them can be determined titrimetrically in the same way. It is also possible to determine the contents of [2.2.1] and [2.2.2] by using a calcium or barium standard solution and the unknown cryptand solution as a titrant. By evaluation of the pH-curve thus obtained, the endpoint of the titration can be determined. In the concentration range of 10−1–10−2 M relative standard deviations of about 0.5% are obtained. [2.2.1] cryptand solutions are determined by using the standard addition technique of Gran with a calcium chloride solution. An ion-selective electrode is used as a probe for calcium ions. If this method is applied, the relative standard deviation in the range of 10−2–10−4 M solutions is approximately 3%. With this technique cryptand can be analysed even when cryptate is present in the solution.
    Notes: Zusammenfassung Bei Verwendung von Bromkresolgrün als visueller Endpunktindicator kann man [2.2.1] und [2.2.2] Kryptandlösungen im Konzentrationsbereich 10−1–10−3 M mit relativen Standardabweichungen von 0,2–0,4% mit HCl titrieren. Wenn in einer Lösung sowohl Kryptand als auch Kryptat vorhanden ist, ist die Summe beider Substanzen auf die gleiche Weise bestimmbar. [2.2.1] und [2.2.2] können auch dadurch bestimmt werden, daß eine Calciumbzw. Barium-Standardlösung mit der Kryptandlösung unbekannter Konzentration titriert wird. Die Auswertung der dabei erhaltenen pH-Kurve ergibt den Titrationsendpunkt, wobei hierdurch im Konzentrationsbereich von 10−1–10−2 M Kryptandlösungen relative Standardabweichungen von etwa 0,5% erreicht werden. [2.2.1] Kryptandlösungen werden außerdem mit der Standard-Additionstechnik nach Gran bestimmt, wobei eine calciumselektive Elektrode als Indicatorelektrode dient. Dabei werden im Konzentrationsbereich von 10−2–10−4 M relative Standardabweichungen von etwa 3 % erhalten. Diese Methode kann auch überschüssigen Kryptand neben Kryptat bestimmen.
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    Titrimetry in a continuous flow system (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 293 (1978), S. 413-415 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Sulfat in Umweltmaterial ; Volumetrie ; Durchflußsystem, Dimethylsulfonazo als Indicator
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00471465
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    Gas-chromatographische Analyse von Kohlenwasserstoffen in der Außenluft nach Probenahme mit dem Tieftemperaturgradientenrohr (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 291 (1978), S. 299-307 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von Kohlenwasserstoffen in Luft ; Chromatographie, Gas ; Tieftemperaturgradientenrohr
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Es wird über ein gas-chromatographisches Verfahren zur Bestimmung von Alkanen, Alkenen und Aromaten in der Außenluft berichtet, bei dem die Probenahme an Tenax GC oder Carbopack mit Hilfe eines Tieftemperaturgradientenrohres erfolgt und die Analyse unter Einsatz eines Doppelsäulensystems in Verbindung mit zwei Flammenionisationsdetektoren durchgeführt wird. Eingehende Untersuchungen zum Verhalten der Substanzen bei der Probenahme zeigen, daß die Trocknung der Probeluft mit Magnesiumperchlorat das Ergebnis nicht beeinflußt und für Kohlenwasserstoffe mit drei oder mehr C-Atomen keine auf Durchbruch zurückzuführenden Substanzverluste zu befürchten sind. Bei einem Probenahmevolumen von 51 Luft können 2 μg Substanz/m3 gut bestimmt werden. Für Außenluft-Konzentrationen von 45 μg Benzol/m3, 95 μg Toluol/m3 und 35 μg n-Pentan/m3 betrugen die Standardabweichungen 3,5, 6,0 bzw. 3,6 μg/m3. Bei leichter Modifikation des Systems ist mit derselben Probenahmevorrichtung die gleichzeitige Bestimmung von Kohlenwasserstoffen mit einem Flammenionisationsdetektor und von Organohalogen Verbindungen mit einem Elektroneneinfangdetektor möglich.
    Notes: Summary A method is described for the gas-chromatographic determination of alkanes, alkenes and aromatics in ambient air. The hydrocarbons are trapped by cryogenic sampling using Tenax GC or Carbopack as adsorbing material and are analyzed in a two-column system equipped with two flame-ionization detectors. A detailed examination of the sampling procedure shows that drying the air with magnesium perchlorate does not affect the results, and losses of substances due to break-through need not be reckoned with for hydrocarbons with three and more carbon atoms. In a 51 air sample 2 μg/m3 of hydrocarbons can be determined readily. The standard deviations for benzene, toluene and n-pentane were 3.5, 6.0 and 3.6 μg/m3 at ambient air concentrations of 45, 95 and 35 μg/m3. A slight modification of the system which includes the combined use of a flame-ionization detector and an electron-capture detector permits the simultaneous determination of hydrocarbons and halogenated hydrocarbons.
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    Gas-chromatographische Kontrolle der Herstellung von Dimethylterephthalat (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 294 (1979), S. 409-409 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von Dimethylterephthalat ; Chromatographie, Gas ; Oxidationsgemisch
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00468536
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    Rapid quantitative gas-chromatographic analysis of 1,3,5-trioxane (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 294 (1979), S. 410-411 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von 1,3,5-Trioxan ; Chromatographie, Gas
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00468538
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    A new analytical system for multicomponent gas-chromatographic analysis of metabolites in biological material (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 292 (1978), S. 39-42 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von Metaboliten in Biolog. Material ; Chromatographie, Gas ; Fraktionierung durch Extraktion
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Summary A new method for the gas-chromatographic multicomponent analysis of metabolites in biological material is described. It is an analytical procedure involving several extractions carried out under different conditions. In this procedure the metabolites are divided according to their functional groups and specific chemical behaviours into eight main fractions: lipids, hydrocarbons, organic acids, neutral substances, phenols, amines, amino acids and carbohydrates. Each of these fractions is derivatized; the components are separated and estimated by gas chromatography. This analytical system was applied to the determination of a number of metabolites in serum, urine, amniotic fluid, sperma, tissues and other biological materials.
    Notes: Zusammenfassung Eine Methode für die Multikomponenten-GC-Analyse von Metaboliten in Biomaterialien wird beschrieben. Das Verfahren umfaßt mehrere Extraktionen, die unter verschiedenen Bedingungen durchgeführt werden. Die Komponenten werden in Abhängigkeit von ihren funktionellen Gruppen und spezifischem chemischen Verhalten in acht Hauptfraktionen geteilt: Lipide, Kohlenwasserstoffe, organische Säuren, neutrale Substanzen, Phenole, Amine, Aminosäuren und Kohlenhydrate. Die Komponenten jeder Gruppe werden nach spezieller Derivatisierung gaschromatographisch getrennt und bestimmt. Dieses neue System ist bei verschiedenen biologischen Materialien (klinische Proben, Pflanzen- und Tiergewebe) angewandt worden.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00481328
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    Über die Zusammensetzung des (1∶2)-Bor-Curcumin-Chelates »Rosocyanin« (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 295 (1979), S. 269-270 
    Details
    ISSN: 1618-2650
    Keywords: Untersuchungen an Bor-Curcumin-Chelaten ; Thermodifferentialanalyse ; Volumetrie ; DMSO
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00481491
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  • 79
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    Bestimmung von Wasserspuren in Chlorcyan durch Karl-Fischer-Titration (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 295 (1979), S. 380-381 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Wasser in Chlorcyan ; Volumetrie ; Karl Fischer, Ethylenglykol
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Es wird eine Methode zur Bestimmung von Wasserspuren in verflüssigtem Chlorcyan beschrieben. Nach Hinzufügen von Chlorcyan zu Ethylenglykol wird das Chlorcyan durch Verdampfen entfernt. Das durch das Ethylenglykol zurückgehaltene Wasser wird mit Karl-Fischer-Lösung titriert. Die Standardabweichungen sind im Bereich von 0,004–0,007 (0,1–0,4 g H2O/100 ml ClCN).
    Notes: Summary A description is given of a method for determining traces of water in liquefied cyanogen chloride. Following the addition to ethylene glycol, cyanogen chloride is removed by evaporation. The water retained by ethylene glycol is then titrated by Karl-Fischer solution. Standard deviations are in the range of 0.004–0.007 (0.1–0.4 g H2O/100 ml ClCN).
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  • 80
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    Fluorspezifischer Detektor für die Gas-Chromatographie (GC) mit Hilfe der Candoluminescenz (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 297 (1979), S. 117-120 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Fluor ; Chromatographie, Gas ; F-spezifischer Detektor, Candoluminescenz
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Es wird ein spektroskopischer fluor-spezifischer Detektor für gas-chromatographische (GC) Anwendungen beschrieben, der sich der Candoluminescenz bedient. Das Auftreten von InF-Bandenemissionen bei 233,7 nm bei Anwendung des MECA (= Molecular Emission Cavity Analysis)-Verfahrens kann als qualitatives Zeichen für die Anwesenheit von F in einer GC-Fraktion benützt werden. Nach entsprechender Kalibrierung kann die Bandenemission als Maß für die F-Konzentration in einer Fraktion dienen. Die Reproduzierbarkeit ist besser als ±2%, die Nachweisgrenze liegt bei 3,2 μg F pro Peak.
    Notes: Summary A fluorine-specific spectroscopical detector is described that takes advantage of candoluminescence. The intensity of the InF-band emission at 233.7 nm in Molecular-Emission-Cavity Analysis (MECA) is an indicator for F in a GC-fraction. After calibration the band intensity can be used as measure for the F-content in the fraction. The reproducibility is better than ±2%, the detection limit 3.2 μg F per peak.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00483590
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  • 81
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    Die Gas-Chromatographische Bestimmung von Spuren niederer Carbon- und Sulfonsäuren in wä\rigen Lösungen (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 292 (1978), S. 385-390 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Carbonsäuren, Sulfonsäuren ; Chromatographie, Gas ; Spuren in wäßrigem Medium
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Gas-chromatographische Methoden für die Spurenbestimmung einiger Carbonund Sulfonsäuren in wäßrigem Medium werden beschrieben. Die Nachweisvermögen für Ameisensäure, Essigsäure, Propionsäure, n-Buttersäure, n-Valeriansäure, Capronsäure, Acrylsäure, Benzoesäure und Chloressigsäure sowie für Methansulfonsäure und Äthansulfonsäure liegen zwischen 1 · 10−7 und 8 · 10−7 Mol/Liter. Anreicherung und Derivatisierung werden bei den Carbonsäuren durch Gefriertrocknung der Tetra-n-butylammoniumsalze und deren Umsetzung mit Benzylbromid zu den Benzylestern, bei den Sulfonsäuren durch Gefriertrocknung der Silbersalze und deren Umsetzung mit n-Butyljodid zu den n-Butylestern erreicht.
    Notes: Summary Gas-chromatographic methods for the determination of traces of several carboxylic and sulphonic acids in aqueous media are presented. Detection limits for formic, acetic, propionic, n-butyric, isobutyric, n-valeric, caproic, acrylic, benzoic, and chloroacetic acids as well as of methanesulphonic and ethanesulphonic acids range from 1 · 10−7 moles/liter to 8 · 10−7 moles/liter. Preconcentration and derivatisation of the carboxylic acids are achieved by freezedrying their tetra-n-butylammonium salts and converting the latter into the benzyl carboxylates using benzyl bromide. The sulphonic acids are converted to the corresponding silver salts, freeze-dried, and then esterified using n-butyl iodide.
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  • 82
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    Delafield's haematoxylin as a new indicator in the nitritometric determination of aromatic primary amines (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 292 (1978), S. 414-414 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Aminen, aromat. primäre ; Volumetrie ; Nitrit, Hämatoxylin als Indicator
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00481568
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  • 83
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    Titrimetry in continuous flow systems (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 298 (1979), S. 155-156 
    Details
    ISSN: 1618-2650
    Keywords: Best. der Alkalität von Umweltmaterial ; Volumetrie ; Durchflußsystem
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00521658
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  • 84
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    Gas-chromatographic determination of traces of acetylsalicylic anhydride and acetylsalicylsalicylic acid in acetylsalicylic acid (1976)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 278 (1976), S. 365-366 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Acetylsalicylsäureanhydrid, Acetylsalicylsalicylsäure in Acetylsalicylsäure ; Chromatographie, Gas
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00531104
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  • 85
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    Zur Anwendung der magnetischen Titration (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 291 (1978), S. 39-41 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Nickel, Jodid ; Volumetrie ; magnetisch, Meßanordnung
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Eine einfache Meßanordnung für die magnetische Titration wird vorgestellt. Anhand der Umsetzung von [Ni(NH3)6]2+ mit CN− und von J− mit Cr2O7 2− wird gezeigt, daß sich dieses Meßverfahren unter bestimmten Voraussetzungen in der quantitativen Analyse einsetzen läßt. Zur Auswertung der Titrationskurven wird eine Auftragung der Kraft im Magnetfeld gegen das reziproke Gesamtvolumen vorgeschlagen.
    Notes: Summary A simple measuring equipment for magnetic titration is described. On the basis of the reaction of [Ni(NH3)6]2+ with CN− and J− with Cr2O7 2− it is shown that under certain conditions this method is useful in quantitative analysis. For evaluation of the titration curves, a plot of the force in the magnetic field against the reciprocal of the total volume is proposed.
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  • 86
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    Identifizierung von Einzelkomponenten in komplexen Gemischen durch Retentions-Index-Vergleich nach Capillar-Gas-Chromatographie mit Elektroneneinfangdetektor (ECD) (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 293 (1978), S. 193-200 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von Umweltmaterial, Pesticiden ; Chromatographie, Gas ; Capillar-, Ident. von Einzelkomponenten in komplexen Gemischen
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Der Vergleich von präzise bestimmten Retentionsindices von Probe- und Referenzsubstanzen in der hochauflösenden Capillar-Gas-Chromatographie stellt eine aussagekräftige Methode der Identifizierung von Einzelkomponenten in komplexen Gemischen dar. Neben der Konstanz der GC-Parameter erfordert die präzise Bestimmung von Retentionsindices eine sehr genaue Bestimmung der Netto-Retentionszeiten. Insbesondere ist bei Anwendung einer Totzeitberechnung auf der Basis einer erzwungenen Linearisierung der log t s/Homologenzahl-Beziehung auf eine sehr genaue Retentionszeitmessung zu achten. Die Reproduzierbarkeit von präzise bestimmten Retentionsindices hängt von der Konstanz der Polarität und von der Adsorptivität der Capillarsäule ab. An ausreichend desaktivierten und konditionierten Hochleistungs-Capillarsäulen (TZ≥40) können unter der Voraussetzung einer Retentionszeit-Meßgenauigkeit von besser als 0,05% Retentionsindices über einen Zeitraum von mehreren Wochen innerhalb ±0,15 Indexeinheiten reproduziert werden. Eine Übertragung des n-Alkan bezogenen Retentionsindex-Konzeptes auf die homologe Reihe der n-Allkyl-trichloracetate (ATA) ermöglicht die Verwendung des Elektroneneinfang-Detektors (ECD) zur präzisen RetentionsindexBestimmung als Methode einer zuverlässigen Identifizierung von Substanzen im Picogrammbereich.
    Notes: Summary High resolution glass-capillary gas chromatography can be used as a powerful identification tool for single components in complex mixtures, when the matching of retention indices of reference compounds with those found in the sample is based on precise measurements. Besides the constancy of the GC-parameters high precision measurements of retention indices require an accurate determination of net retention times. Special care has to be taken for an accurate measurement of retention times when using a dead-time calculation on the basis of an enforced linearisation of the log t s/homologues-number relationship. The reproducibility of precise retention-index determinations strongly depends on the constancy of the polarity and on the adsorptivity of the capillary column. Provided a sufficiently deactivated and conditioned high performance capillary column (separation number ≥40) and an accuracy of retention-time measurement of better than 0,05 % retention indices can be reproduced within ±0.15 i.u. over a period of several weeks. A conversion of the n-alkane based retention-index concept to the use of the homologous series of n-alkyl-trichloro-acetates (ATA) allows the use of the electron-capture detector (ECD) for precise retention-index determinations for a reliable identification of compounds in the picogram range.
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    URL: http://dx.doi.org/10.1007/BF00491046
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    Gas-chromatographische Kontrolle der Herstellung von Dimethylterephthalat (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 293 (1978), S. 412-413 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von Dimethylterephthalat in Wasser ; Chromatographie, Gas ; Abwasser
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00471464
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  • 88
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    Anreicherung und Nachweis polycyclischer aromatischer Kohlenwasserstoffe in Wasser (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 294 (1979), S. 385-390 
    Details
    ISSN: 1618-2650
    Keywords: Nachw. von Kohlenwasserstoffen, aromat. polycycl. in Wasser ; Chromatographie, Gas ; ECD, Anreicherungsverfahren
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Ein einfaches und schnelles Adsorptionsverfahren zur Anreicherung von polycyclischen aromatischen Kohlenwasserstoffen (=PAK) wird angegeben: nach einer Magnesiumhydroxidfällung in der Wasserprobe wird der Niederschlag abzentrifugiert und durch Zugabe von Ammoniumchlorid gelöst; die organischen Substanzen in dieser Lösung werden mit sehr wenig Cyclohexan extrahiert, wodurch eine Einengung des Extraktes nicht erforderlich ist. Die PAK im Extrakt werden gas-chromatographisch mit ECD-Detektion getrennt. Ein Vergleich dieser neuen Methode mit der “rapid liquid extraction” wird beschrieben.
    Notes: Summary A simple and rapid adsorption method for the enrichment of polycyclic aromatic hydrocarbons (=PAH)is described: after precipitation of magnesium hydroxide in the water sample the precipitate is separated by centrifugation and then dissolved by adding ammonium chloride; the organic substances in this solution are extracted with a very small volume of cyclohexane. A concentration of the extract is not necessary. The PAH in the extract are, separated gaschromatographically using ECD detection. The new method is compared with the “rapid liquid extraction” method.
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    Vollautomatische titrimetrische Einzelanalyse in der Praxis (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 297 (1979), S. 126-131 
    Details
    ISSN: 1618-2650
    Keywords: Volumetrie ; Einzelproben, automatisches Analysengerät
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Voraussetzungen einer effektiven Automation der individuellen titrimetrischen Analyse werden dargestellt. Ein nach diesen Gesichtspunkten entwickeltes Gerät wird beschrieben und seine Anwendung in den Gebieten der Farbstoffe, Agrochemikalien, Additiven und Pharmaka aufgezeigt.
    Notes: Summary Criteria for effective automation of individual titrimetric analyses are presented. Based on these, an automatic titration system has been developed which is described. Its performance and its applicability in the field of dyestuffs, agrochemicals, additives and pharmaceuticals has been investigated.
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    Volumetric determination of strontium in strontium ferrites (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 297 (1979), S. 159-159 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Strontium in Strontiumferriten ; Volumetrie ; Ausfällung bzw. Maskierung von Eisen
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00483598
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  • 91
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    Quantitative Mikrobestimmung von Chlorid (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 298 (1979), S. 43-43 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Chlorid ; Volumetrie ; Dithizon, AgCl
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00470049
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  • 92
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    Abtrennung von Barbitursäurederivaten und Phenytoin aus Harn als schwerlösliche Quecksilber-Verbindungen zur gas-chromatographischen Analyse (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 298 (1979), S. 45-46 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Barbituraten, Phenytoin in Harn ; Chromatographie, Gas ; Hg-Verbindungen v. Barbituraten
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00470051
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    Gas-chromatographische Elementanalyse über Di(trifluoräthyl)dithiocarbamatochelate (1978)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 293 (1978), S. 11-15 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Blei neben Wismut ; Chromatographie, Gas ; Di(trifluoräthyl)dithiocarbamat. — Verhalten von Kupfer(II), Nickel(II), Kobalt(III), Eisen(III), Wismut(III), Blei(II), Antimon(III) ; Verteilung zwischen wäßriger Lösung und Chloroform
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Das Verteilungsverhalten der oben genannten Di(trifluroäthyl)dithiocarbamato-Chelate zwischen wäßrigen Lösungen und Chloroform wird untersucht. Eine Anwendung zur gleichzeitigen gaschromatographischen Bestimmung von Blei und Wismut im ppm-Bereich (0,2–3 ppm) nach Ausschütteln aus wäßrigen Lösungen wird beschrieben (Säule: 5 % GE SE50 auf Gas Chrom Q; 180–240° C; 4°/min; Einspritzblock: 240° C).
    Notes: Summary The solvent extraction of the above di(trifluoroethyl)dithiocarbamatochelates with chloroform is investigated. An application for the simultaneous gas-chromatographic determination 0.2–3 ppm of lead and bismuth after extraction out of aqueous solutions is reported (column: 5% GE SE 50 on Gas Chrom Q; 180–240° C; 4°/min; injection block: 242°C).
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    Direct oxidimetric determination of indigo with vanadate (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 298 (1979), S. 159-159 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Indigo und Vanadat ; Volumetrie ; photometr. Endpunkt
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00521663
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    Zerstörungsfreie Ultramikroanalyse archäologischer Fundstücke (1979)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 298 (1979), S. 269-272 
    Details
    ISSN: 1618-2650
    Keywords: Analyse von Bronze in archäolog. Material ; Volumetrie ; Korundstäbchen
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung In Fortsetzung einer früheren Arbeit über Kupfer und Messing wird in dieser Mitteilung die Zinnbestimmung in Abstrichen beschrieben. Metazinnsäure wird durch Filtration mit Hilfe eines besonderen Gerätes abgetrennt, zu SnS2 umgesetzt, in HCl gelöst und die Sn-Bestimmung wird dann durch Rücktitration eines EDTA-Überschusses mit Zinksulfat durchgeführt.
    Notes: Summary In continuation of an earlier paper on copper and brass this communication describes the determination of tin in streak samples. Metastannic acid is isolated by filtration using a specially designed apparatus. It is converted to SnS2, dissolved in HCl and Sn is determined by back-titration of excess EDTA with zink sulphate.
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    Pantolacton aus Coenzym A. Bestimmung von Pantothensäure (1975)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 277 (1975), S. 124-124 
    Details
    ISSN: 1618-2650
    Keywords: Pantothensäure, Pantolacton ; Chromatographie, Gas ; Hydrolyse von Coenzym A
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00602082
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    Ermittlung des Vernetzungsgrades und Beladungszustandes von Ionenaustauschern auf Kunstharzbasis durch Pyrolyse-Gas-Chromatographie (1975)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 277 (1975), S. 9-17 
    Details
    ISSN: 1618-2650
    Keywords: Ermittlung des Vernetzungsgrades, Beladungszustandes von Ionenaustauschern ; Chromatographie, Gas ; Pyrolyse, Kunstharzbasis
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Zur besseren Reproduzierbarkeit der Zusammensetzung des Pyrolysates bei der Pyrolyse-Gas-Chromatographie wird eine spezielle Eingabenanordnung mit Trägergasumschaltung beschrieben und deren Einfluß auf die Bildung der Pyrolyseprodukte und auf die Retentionszeiten mit einer Modellsubstanz untersucht. Mit Hilfe der Trägergasumschaltung kann man die Bandenflächenverhältnisse zur Bestimmung des Vernetzungsgrades von Ionenaustauschern auf Styrol-DVB-Basis wesentlich genauer ermitteln. Da bei der Pyrolyse von Anionenaustauschern wenigerα-MSt auftritt als bei den Kationenaustauschern, sind die Bandenflächenverhältnisse bei ersteren wesentlich größer. Bei den Anionenaustauschern werden sie mit steigendem Vernetzungsgrad kleiner, wohingegen bei den Kationenaustauschern die Werte steigen. Bei 400° C erfolgt der thermische Angriff im wesentlichen an der aktiven Gruppe der Anionenaustauscher mit Styrol-DVB-Matrix. Die aus dem Gegenion entstehenden Methylester bzw. deren Zersetzungsprodukte sind charakteristische Pyrolyseprodukte. Kennzeichnend für Dowex 1 ist das Auftreten von Trimethylamin, für Dowex 2 das von Acetaldehyd. Somit ist es mit der Pyrolyse-Gas-Chromatographie möglich, zusätzlich zur Matrix, Art und Struktur der funktionellen Gruppe sowie Substitutionsstelle der Ankergruppen an der Matrix auch Vernetzungsgrad und Beladungszustand von Ionenaustauschern zu ermitteln.
    Notes: Abstract A special introduction device with switching of carrier gas for improving the reproducibility of pyrolysate composition in pyrolysis gas-chromatography has been described. Its influence on the formation of pyrolysis products and on retention times has been studied on a model substance. The peak area ratios for determining the degree of cross-linking in ion exchangers on styrene-DVB basis can be estimated considerably more accurately with the help of carrier gas switching. Since anion exchangers yield lessα-methylstyrene on pyrolysis than do cation exchangers, their peak area ratios are appreciably larger. Increasing the degree of cross-linking lowers the ratios with the anion exchangers and raises them with the cation exchangers. At 400° C the thermal attack on anion exchangers with styrene-DVB matrix occurs mainly at the active group. The methyl esters or their decomposition products formed from the counter ions are characteristic pyrolysis products. A feature of Dowex 1 is the formation of trimethylamine; of Dowex 2, acetaldehyde. In this way, pyrolysis gas-chromatography enables information about the degree of cross linking and the nature of the anion of ion exchangers, as well as about the matrix, type and structure of the functional group and position of substitution of the anchor group in the matrix to be obtained.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00591870
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    Direct volumetric determination of sulphonamides by bromination with N-bromosuccinimide (1975)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 277 (1975), S. 125-125 
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    ISSN: 1618-2650
    Keywords: Sulfonamiden mit N-Bromsuccinimid ; Volumetrie
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00602083
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    Ultrapolare Mischphasen zur GLC-Bestimmung von Benzol (1975)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 277 (1975), S. 31-32 
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    ISSN: 1618-2650
    Keywords: Best. von Benzol ; Chromatographie, Gas ; ultrapolare Mischphasen
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00591874
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    Field method for the volumetric determination of fluoride in water using SPADNS and thorium nitrate (1975)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 277 (1975), S. 207-207 
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    ISSN: 1618-2650
    Keywords: Best. von Fluorid in Wasser ; Volumetrie ; SPADNS und Thoriumnitrat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00462241
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