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  • ddc:550.78  (32)
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  • 1
    Publication Date: 2024-04-03
    Description: To complement the information provided by deterministic seismic imaging at length scales above a certain resolution limit we present the first application of adjoint envelope tomography (AET) to experimental data. AET uses the full envelopes of seismic records including scattered coda waves to obtain information about the distribution of absorption and small‐scale heterogeneity which provide complementary information about the investigated medium. Being below the resolution limit this small‐scale structure cannot be resolved by conventional tomography but still affects wave propagation by attenuating ballistic waves and generating scattered waves. Using ultrasound data from embedded sensors in a meter‐sized concrete specimen we image the distribution of absorption and heterogeneity expressed by the intrinsic quality factor Q〈sup〉−1〈/sup〉 and the fluctuation strength ɛ that characterizes the strength of the heterogeneity. The forward problem is solved by modeling the 2‐D multiple nonisotropic scattering in an acoustic medium with spatially variable heterogeneity and attenuation using the Monte‐Carlo method. Gradients for the model updates are obtained by convolution with the back‐propagated envelope misfit using the adjoint formalism in analogy to full waveform inversion. We use a late coda time window to invert for absorption and an earlier time window to infer the distribution of heterogeneity. The results successfully locate an area of salt concrete with increased scattering and concentric anomalies of intrinsic attenuation. The resolution test shows that the recovered anomalies constitute reasonable representations of internal structure of the specimen.
    Description: Plain Language Summary; No matter how small the structures are that a seismic imaging method is able to resolve, there is structure with smaller length scale. On the one hand this small‐scale structure causes unwanted signals for conventional imaging approaches. But on the other hand it provides complementary information about the investigated medium. To turn this to our advantage we, for the first time, apply a new imaging method that uses the waves which are caused by the small‐scale structure. Using data of an experiment in a concrete block we demonstrate that we can identify areas of anomalous small‐scale structure. The results may help in the future to locate minute perturbations in the medium as they occur in the advent of volcanic eruptions or after earthquakes and to obtain new information about the geologic history of subsurface materials. The approach can be transferred to investigate man‐made materials and structures, such as deteriorating concrete constructions.
    Description: Key Points: Adjoint envelope tomography is for the first time applied to image the scattering and absorption structure with the real data. The iterative inversion uses envelopes of ultrasound signals from embedded transducers in a meter‐sized reinforced concrete specimen. We successfully image the distribution of statistical parameters characterizing the small‐scale heterogeneity and attenuation.
    Description: China Scholarship Council http://dx.doi.org/10.13039/501100004543
    Description: https://doi.org/10.5281/zenodo.7152278
    Keywords: ddc:550.78 ; seismic tomography ; adjoint method ; small‐scale heterogeneity ; attenuation ; ultrasonic experiment ; reinforced concrete
    Language: English
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  • 2
    Publication Date: 2024-03-25
    Description: This study aims to experimentally investigate the possibility of combining two extended continuum theories for two‐phase flow. One of these theories considers interfacial area as a separate state variable, and the other explicitly discriminates between connected and disconnected phases. This combination enhances our potential to effectively model the apparent hysteresis, which generally dominates two‐phase flow. Using optical microscopy, we perform microfluidic experiments in quasi‐2D artificial porous media for various cyclic displacement processes and boundary conditions. Specifically for a number of sequential drainage processes, with detailed image (post‐)processing, pore‐scale parameters such as the interfacial area between the phases (wetting, non‐wetting, and solid), and local capillary pressure, as well as macroscopic parameters like saturation, are estimated. We show that discriminating between connected and disconnected clusters and the concept of the interfacial area as a separate state variable can be an appropriate way of modeling hysteresis in a two‐phase flow scheme. The drainage datasets of capillary pressure, saturation, and specific interfacial area, are plotted as a surface, given by f (P〈sup〉c〈/sup〉, s〈sup〉w〈/sup〉, a〈sup〉wn〈/sup〉) = 0. These surfaces accommodate all data points within a reasonable experimental error, irrespective of the boundary conditions, as long as the corresponding liquid is connected to its inlet. However, this concept also shows signs of reduced efficiency as a modeling approach in datasets gathered through combining experiments with higher volumetric fluxes. We attribute this observation to the effect of the porous medium geometry on the phase distribution. This yields further elaboration, in which this speculation is thoroughly studied and analyzed.
    Description: Key Points: A large number of two‐phase displacement microfluidic experiments under different boundary conditions are performed. A code has been developed in order to spatially and temporally resolve the experiments with high accuracy. Including both connectivity and interfacial area as state variables in two‐phase flow continuum theories improves modeling hysteresis.
    Description: Deutsche Forschungsgemeinschaft http://dx.doi.org/10.13039/501100001659
    Description: Stuttgart Center for Simulation Science, Universität Stuttgart http://dx.doi.org/10.13039/501100022175
    Description: https://doi.org/10.18419/darus-2250
    Keywords: ddc:550.78 ; microfluidic experiments ; optical microscopy ; two‐phase flow in porous medium ; image processing ; extended theory of porous medium ; phase connectivity
    Language: English
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  • 3
    Publication Date: 2024-02-14
    Description: 〈title xmlns:mml="http://www.w3.org/1998/Math/MathML"〉Abstract〈/title〉〈p xmlns:mml="http://www.w3.org/1998/Math/MathML" xml:lang="en"〉Aseismic slip may occur during a long preparatory phase preceding earthquakes, and what controls it remains poorly understood. In this study, we explored the role of load point velocity and surface roughness on slow slip during the preparatory stage prior to stick‐slip events. To that end, we conducted displacement‐rate controlled friction experiments by imposing varying load point velocities on sawcut granite samples with different surface roughness at a confining pressure of 35 MPa. We measured the average slip along the fault with the recorded far‐field displacements and strain changes, while acoustic emission sensors and local strain gages were used to capture local slip variations. We found that the average amount of aseismic slip during the preparatory stage increases with roughness, whereas precursory slip duration decreases with increased load point velocity. These results reveal a complex slip pattern on rough faults which leads to dynamic ruptures at high load point velocities.〈/p〉
    Description: Plain Language Summary: Earthquakes occur mostly along preexisting faults in the earth crust. These faults exhibit various geometrical complexities and are subjected to different strain rates. In the laboratory, we produce earthquake analogs by sliding sawcut granite blocks. We vary the geometrical complexity of the faults by roughening their surfaces and modify the strain rate by displacing the blocks at varying velocities. Under these different conditions, we measure how the forces accumulated by friction are released, by measuring stresses and displacements applied on the block's edges, using local strain deformation sensors, and by recording very small earthquakes occurring during sliding along the sawcut faults. We find that smooth sawcut faults tend to release all the energy accumulated very abruptly, after a very small amount of slip, regardless of the load point velocity applied. The processes leading to failure in the case of a rough fault are much more complex, involving a large amount of slip, and numerous small earthquakes which are distributed heterogeneously in space and time.〈/p〉
    Description: Key Points: 〈list list-type="bullet"〉 〈list-item〉 〈p xml:lang="en"〉Acoustic emissions highlight the complex preparatory phase prior stick‐slips on rough faults〈/p〉〈/list-item〉 〈list-item〉 〈p xml:lang="en"〉Preparatory slip increases with roughness and the duration of the preparatory phase decreases with increasing load point velocity〈/p〉〈/list-item〉 〈list-item〉 〈p xml:lang="en"〉Rough and heterogeneous faults are more stable than smooth faults, but can become unstable with a small increase of load point velocity〈/p〉〈/list-item〉 〈/list〉 〈/p〉
    Description: SAIDAN
    Description: https://doi.org/10.5281/zenodo.6411819
    Keywords: ddc:550.78 ; rock friction ; roughness ; dynamic rupture ; acoustic emissions
    Language: English
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  • 4
    Publication Date: 2023-12-19
    Description: The paper presents an experimental study on the effect of plastic fines content on the undrained behavior and liquefaction susceptibility of sand–fines mixtures under monotonic loading. The results of undrained monotonic triaxial compression tests conducted on mixtures of Hostun sand with varying amount (0–20%) and type (kaolin and calcigel bentonite) of plastic fines are presented. The specimens were prepared with different initial densities using the moist tamping method and consolidated at two different isotropic effective stresses. The results demonstrate that for both types of plastic fines, an increase in the fines content leads to a more contractive response and lower values of mobilized deviatoric stress. Despite similar relative density and fines content, the sand–kaolin mixtures showed a more contractive behavior than the sand–calcigel specimens. The steady-state lines (SSLs) in e–p´ space generally move downwards with increasing clay content. While the slopes of the SSLs for the clean Hostun sand and the mixtures with 10 and 20% kaolin are quite similar, the SSL lines for the specimens containing 10% or 20% calcigel run steeper or flatter, respectively. The inclination of the SSL in the q–p′ plane was found independent of clay type and content. The sand–kaolin mixtures were observed to be more susceptible to instability and flow liquefaction than the sand–calcigel mixtures.
    Keywords: ddc:550.78 ; Instability line ; Plastic fines content ; Sand–fines mixtures ; Steady-state line ; Undrained monotonic triaxial tests
    Language: English
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  • 5
    Publication Date: 2023-11-17
    Description: 〈p xmlns:mml="http://www.w3.org/1998/Math/MathML" xml:lang="en"〉Laser ablation multi‐collector‐inductively coupled plasma‐mass spectrometry (LA‐MC‐ICP‐MS) has become a valuable tool for the 〈italic toggle="no"〉in situ〈/italic〉 measurement of the boron isotope composition of geological samples at high (tens to hundreds of μm) spatial resolution. That said, this application suffers from significant analytical challenges. We focus in this study on the underlying processes of two of the main causes for inaccuracies using this technique. We provide empirical evidence that not only Ca ions (Sadekov 〈italic〉et al〈/italic〉. 2019, Standish 〈italic〉et al〈/italic〉. 2019, Evans 〈italic〉et al〈/italic〉. 2021) but also Ar ions, that are reflected within the flight tube of the mass spectrometer, are the source for previously reported issues with spectral baselines. We also address the impact of plasma conditions on the instrumental mass fractionation as a source for matrix‐ and mass‐load‐related analytical biases. Comparing experimental data with the results of a dedicated release and diffusion model (RDM) we estimate that a close to complete (~ 97%) release of boron from the sample aerosol is needed to allow for consistently accurate LA boron isotope measurement results without the need for corrections.〈/p〉
    Description: Key Points: 〈list list-type="bullet" id="ggr12500-list-0101"〉 〈list-item〉〈p〉Two separate main sources for inaccuracy of boron isotope measurements by laser ablation: B isotope fractionation in the ICP and the known scattered ion baseline problem.〈/p〉〈/list-item〉 〈list-item〉〈p〉Boron isotope fractionation in the ICP varies systematically with plasma condition (NAI).〈/p〉〈/list-item〉 〈list-item〉〈p〉Behaviour of B isotopes within the ICP simulated by a release and diffusion model (RDM).〈/p〉〈/list-item〉 〈/list〉 〈boxed-text position="anchor" content-type="graphic" id="ggr12511-blkfxd-0001" xml:lang="en"〉 〈graphic position="anchor" id="jats-graphic-1" xlink:href="urn:x-wiley:16394488:media:ggr12511:ggr12511-toc-0001"〉 〈/graphic〉 〈/boxed-text〉 〈/p〉
    Keywords: ddc:550.78 ; boron isotopes ; laser ablation ; scattered ions ; mass fractionation ; plasma conditions
    Language: English
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  • 6
    Publication Date: 2023-11-16
    Description: This research work presents an experimental and numerical study of the coupled thermo-hydro-mechanical (THM) processes that occur during soil freezing. With focusing on the artificial ground freezing (AGF) technology, a new testing device is built, which considers a variety of AGF-related boundary conditions and different freezing directions. In the conducted experiments, a distinction is made between two thermal states: (1) The thermal transient state, which is associated with ice penetration, small deformations, and insignificant water suction. (2) The thermal (quasi-) steady state, which has a much longer duration and is associated with significant ice lens formation due to water suction. In the numerical modeling, a special focus is laid on the processes that occur during the thermal transient state. Besides, a demonstration of the micro-cryo-suction mechanism and its realization in the continuum model through a phenomenological retention-curve-like formulation is presented. This allows modeling the ice lens formation and the stiffness degradation observed in the experiments. Assuming a fully saturated soil as a biphasic porous material, a phase-change THM approach is applied in the numerical modeling. The governing equations are based on the continuum mechanical theory of porous media (TPM) extended by the phase-field modeling (PFM) approach. The model proceeds from a small-strain assumption, whereas the pore fluid can be found in liquid water or solid ice state with a unified kinematics treatment of both states. Comparisons with the experimental data demonstrate the ability and usefulness of the considered model in describing the freezing of saturated soils.
    Description: Deutsche Forschungsgemeinschaft http://dx.doi.org/10.13039/501100001659
    Description: RWTH Aachen (3131)
    Keywords: ddc:550.78 ; Experimental study ; Frost heave ; Ice lens formation ; Phase-field modeling ; Soil freezing ; Thermo-hydro-mechanical coupling
    Language: English
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  • 7
    Publication Date: 2023-11-15
    Description: The hydromechanical properties of single self-propping fractures under stress are of fundamental interest for fractured-rock hydrology and a large number of geotechnical applications. This experimental study investigates fracture closure and hydraulic aperture changes of displaced tensile fractures, aligned tensile fractures, and saw-cut fractures for two types of sandstone (i.e., Flechtinger and Fontainebleau) with contrasting mechanical properties, cycling confining pressure between 5 and 30 MPa. Emphasis is placed on how surface roughness, fracture wall offset, and the mechanical properties of the contact asperities affect the self-propping potential of these fractures under normal stress. A relative fracture wall displacement can significantly increase fracture aperture and hydraulic conductivity, but the degree of increase strongly depends on the fracture surface roughness. For smooth fractures, surface roughness remains scale-independent as long as the fracture area is larger than a roll-off wavelength and thus any further displacement does not affect fracture aperture. For rough tensile fractures, these are self-affine over a larger scale so that an incremental fracture wall offset likely leads to an increase in fracture aperture. X-ray microtomography of the fractures indicates that the contact area ratio of the tensile fractures after the confining pressure cycle inversely correlates with the fracture wall offset yielding values in the range of about 3–25%, depending, first, on the respective surface roughness and, second, on the strength of the asperities in contact. Moreover, the contact asperities mainly occur isolated and tend to be preferentially oriented in the direction perpendicular to the fracture wall displacement which, in turn, may induce flow anisotropy. This, overall, implies that relatively harder sedimentary rocks have a higher self-propping potential for sustainable fluid flow through fractures in comparison to relatively soft rocks when specific conditions regarding surface roughness and fracture wall offset are met.
    Description: Bundesministerium für Wirtschaft und Energie (DE)
    Description: China Scholarship Council http://dx.doi.org/10.13039/501100004543
    Description: Helmholtz-Zentrum Potsdam Deutsches GeoForschungsZentrum - GFZ (4217)
    Keywords: ddc:550.78 ; Self-propping fracture ; Mechanical aperture ; Hydraulic aperture ; Normal stress ; Fracture wall offset ; Surface roughness
    Language: English
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  • 8
    Publication Date: 2023-11-15
    Description: Using an innovative experimental set-up (Punch-Through Shear test), we initiated a shear zone (microfault) in Flechtingen sandstone and Odenwald granite under in situ reservoir conditions while monitoring permeability and fracture dilation evolution. The shear zone, which has a cylindrical geometry, is produced by a self-designed piston assembly that punches down the inner part of the sample. Permeability and fracture dilation were measured for the entire duration of the experiment. After the shear zone generation, the imposed shear displacement was increased to 1.2 mm and pore pressure changes of ±5 or ±10 MPa were applied cyclically to simulate injection and production scenarios. Thin sections and image analysis tools were used to identify microstructural features of the shear zone. The geometry of the shear zone is shown to follow a self-affine scaling invariance, similar to the fracture surface roughness. The permeability evolution related to the onset of the fracture zone is different for both rocks: almost no enhancement for the Flechtingen sandstone and an increase of more than 2 orders of magnitude for the Odenwald granite. Further shear displacement resulted in a slight increase in permeability. A fault compaction is observed after shear relaxation which is associated to a permeability decrease by a factor more than 3. Permeability changes during pressure cycling are reversible when varying the effective pressure. The difference in permeability enhancement between the sandstone and the granite is related to the larger width of the shear zones.
    Description: ReSalt Project
    Description: H2020 European Research Council http://dx.doi.org/10.13039/100010663
    Description: Projekt DEAL
    Keywords: ddc:550.78 ; Microfault ; Fracture permeability ; Microstructure ; Fault architecture ; Roughness ; Sandstone ; Granite
    Language: English
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  • 9
    Publication Date: 2023-11-15
    Description: In this work, we aim to verify the predictions of the numerical simulators, which are used for designing field-scale hydraulic stimulation experiments. Although a strong theoretical understanding of this process has been gained over the past few decades, numerical predictions of fracture propagation in low-permeability rocks still remains a challenge. Against this background, we performed controlled laboratory-scale hydraulic fracturing experiments in granite samples, which not only provides high-quality experimental data but also a well-characterized experimental set-up. Using the experimental pressure responses and the final fracture sizes as benchmark, we compared the numerical predictions of two coupled hydraulic fracturing simulators—CSMP and GEOS. Both the simulators reproduced the experimental pressure behavior by implementing the physics of Linear Elastic Fracture Mechanics (LEFM) and lubrication theory within a reasonable degree of accuracy. The simulation results indicate that even in the very low-porosity (1–2 %) and low-permeability (10〈sup〉−18〈/sup〉 m〈sup〉2〈/sup〉 − 10〈sup〉−19〈/sup〉 m〈sup〉2〈/sup〉) crystalline rocks, which are usually the target of EGS, fluid-loss into the matrix and unsaturated flow impacts the formation breakdown pressure and the post-breakdown pressure trends. Therefore, underestimation of such parameters in numerical modeling can lead to significant underestimation of breakdown pressure. The simulation results also indicate the importance of implementing wellbore solvers for considering the effect of system compressibility and pressure drop due to friction in the injection line. The varying injection rate as a result of decompression at the instant of fracture initiation affects the fracture size, while the entry friction at the connection between the well and the initial notch may cause an increase in the measured breakdown pressure.
    Description: European Union's Horizon 2020 Research and Innovation programme
    Description: Commonwealth Scientific and Industrial Research Organisation http://dx.doi.org/10.13039/501100000943
    Description: RWTH Aachen (3131)
    Description: http://doi.org/10.5281/zenodo.3710746
    Keywords: ddc:550.78 ; Laboratory-experiments ; Hydraulic fracturing ; Simulation ; Leak-off ; Fracture toughness ; System compressibility ; Fracture radius ; Acoustic emission
    Language: English
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  • 10
    Publication Date: 2023-11-15
    Description: This is a repond to the comments raised in Crisci´s et al. paper “Discussion on “Experimental Deformation of Opalinus Clay at Elevated Temperature and Pressure Conditions ¬ Mechanical Properties and the Influence of Rock Fabric” (2021). We are pleased to use the opportunity to clarify issues related to testing procedures and interpretation in more detail.
    Description: Bundesministerium für Bildung und Forschung http://dx.doi.org/10.13039/501100002347
    Description: Helmholtz-Gemeinschaft http://dx.doi.org/10.13039/501100001656
    Description: Helmholtz-Zentrum Potsdam Deutsches GeoForschungsZentrum - GFZ (4217)
    Keywords: ddc:550.78 ; Opalinus Clay ; Testing procedure ; Pore pressure generation ; Strain rate ; Drying-induced micro cracks
    Language: English
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