Signatur:
M 21.94523
Materialart:
Monographie ausleihbar
Seiten:
528 Seiten
,
Illustrationen, Diagramme
,
26 cm x 16.5 cm
Ausgabe:
5th revised edition
ISBN:
9783866305328
,
386630532X
Serie:
European coatings library
Originaltitel:
Das Rheologie-Handbuch 〈engl〉
URL:
https://d-nb.info/1216579180/04
Sprache:
Englisch
Anmerkung:
Contents
1. Introduction
1.1 Rheology, rheometry and viscoelasticity
1.2 Deformation and flow behavior
1.3 References
2 Flow behavior and viscosity
2.1 Introduction
2.2 Definition of terms
2.2.1 Shear stress
2.2.2 Shear rate
2.2.3 Viscosity
2.3 Shear load-dependent flow behavior
2.3.1 Ideal-viscous flow behavior
2.4 Types of flow illustrated by the Two-Plates model
2.5 References
3 Rotational tests
3.1 Introduction
3.2 Basic principles
3.2.1Test modes-controlled shear rate (CSR) and controlled shear stress (CSS), raw data and rheological parameters
3.3 Flow curves and viscosity functions
3.3.1 Description of the test
3.3.2 Shear-thinning flow behavior
3.3.3 Shear-thickening flow behavior
3.3.4 Yield point
3.3.5 Overview: flow curves and viscosity functions
3.3.6 Fitting functions for flow and viscosity curves
3.3.7 The effects of rheology additives in water-based dispersions
3.4 Time-dependent flow behavior and viscosity function
3.4.1 Test description
3.4.2 Time-dependent flow behavior of samples showing no hardening
3.4.3 Time-dependent flow behavior of samples showing hardening
3.5 Temperature-dependent flow behavior and viscosity function
3.5.1 Test description
3.5.2 Temperature-dependent flow behavior of samples showing no hardening
3.5.3 Temperature-dependent flow behavior of samples showing hardening
3.5.4 Fitting functions for curves of the temperature-dependent viscosity
3.6 Pressure-dependent flow behavior and viscosity function
3.7 References
4 Elastic behavior and shear modulus
4.1 Introduction
4.2 Definition of terms
4.2.1 Deformation and strain
4.2.2 Shear modulus
4.3 Shear load-dependent deformation behavior
4.3.1 Ideal-elastic deformation behavior
4.4 Yield point determination using the shear stress/deformation diagram
4.5 References
5 Viscoelastic behavior
5.1 Introduction
5.2 Basic principles
5.2.1 Viscoelastic liquids according to Maxwell
5.2.2 Viscoelastic solids according to Kelvin/Voigt
5.3 Normal stresses
5.4 References
6 Creep tests
6.1 Introduction
6.2 Basic principles
6.2.1 Description of the test
6.2.2 Ideal-elastic behavior
6.2.3 Ideal-viscous behavior
6.2.4 Viscoelastic behavior
6.3 Analysis
6.3.1 Behavior of the molecules
6.3.2 The Burgers model
6.3.3 Curve discussion
6.3.4 Definition of terms
6.3.5 Data conversion
6.3.6 Determination of the molar mass distribution
6.4 Determination of the yield point via creep tests
6.5 References
7 Relaxation tests
7.1 Introduction
7.2 Basic principles
7.2.1 Description of the test
7.2.2 Ideal-elastic behavior
7.2.3I deal-viscous behavior
7.2.4 Viscoelastic behavior
7.3 Analysis
7.3.1 Behavior of the molecules
7.3.2 Curve discussion
7.3.3 Definition of terms
7.3.4 Data conversion
7.3.5 Determination of the molar mass distribution
7.4 References
8 Oscillatory tests
8.1 Introduction
8.2 Basic principles
8.2.1 Ideal-elastic behavior
8.2.2 Ideal-viscous behavior
8.2.3 Viscoelastic behavior
8.2.4 Definition of terms
8.2.5 The test modes controlled shear strain and controlled shear stress, raw data and rheological parameters
8.3 Amplitude sweeps
8.3.1 Description of the test
8.3.3 Limiting value of the LVE range
8.3.4 Determination of the yield point and the flow point by amplitude sweeps
8.3.5 Frequency-dependence of amplitude sweeps
8.3.6 SAGS and LAOS tests, and Lissajous diagrams
8.4 Frequency sweeps
8.4.1 Description of the test
8.4.2 Behavior of uncrosslinked polymers (solutions and melts)
8.4.3 Behavior of crosslinked polymers5
8.4.4 Behavior of dispersions and gels
8.4.5 Comparison of superstructures using frequency sweeps
8.4.6 Multiwave test
8.4.7 Data conversion
8.5 Time-dependent behavior at constant dynamic-mechanical and isothermal conditions
8.5.1 Description of the test
8.5.2 Time-dependent behavior ofs amples showing no hardening
8.5.3 Time-dependent behavior of samples showing hardening
8.6 Temperature-dependent behavior at constant dynamic mechanical conditions
8.6.1 Description of the test
8.6.2 Temperature-dependent behavior of samples showing no hardening
8.6.3 Temperature-dependent behavior of samples showing hardening
8.6.4 Thermoanalysis (TA)
8.7 Time/temperature shift
8.7.1 Temperature shift factor according to the WLF method
8.8 The Cox/Merz relation
8.9 Combined rotational and oscillatory tests
8.9.1 Presetting rotation and oscillation in series
8.9.2 Superposition of oscillation and rotation
8.10 References
9 Complex behavior, surfactant systems
9.1 Surfactant systems
9.1.1 Surfactant structures and micelles
9.1.2 Emulsions
9.1.3 Mixtures of surfactants and polymers, polymers containing surfactant components
9.1.4 Applications of surfactant systems
9.2 Rheological behavior of surfactant systems
9.2.1 Typical shear behavior
9.2.2 Shear-induced effects, shear-banding and "rheochaos"
9.3 References
10 Measuring systems
10.1 Introduction
10.2 Concentric cylinder measuring systems (CCMS)
10.2.1 Cylinder measuring systems in general
10.2.2 Narrow-gap concentric cylinder measuring systems according to ISO3219
10.2.3 Double-gap measuring systems (DCMS)
10.2.4 High-shear cylinder measuring systems (HSMS)
10.3 Cone-and-plate measuring systems (CPMS)
10.3.1 Geometry
10.3.2 Calculations
10.3.3 Conversion between raw data and rheological parameters
10.3.4 Flow instabilities and secondary flow effects in CP systems
10.3.5 Cone truncation and gap setting
10.3.6 Maximum particle size
10.3.7 Filling of the cone-and-plate measuring system
10.3.8 Advantages and disadvantages of cone-and-plate measuring systems
10.4 Parallel-plate measuring systems (PPMS)
10.4.1 Geometry
10.4.2 Calculations
10.4.3 Conversion between raw data and rheological parameters
10.4.4 Flow instabilities and secondary flow effects in a PP system
10.4.5 Recommendations for gap setting
10.4.6 Automatic gap setting and automatic gap control using the normal force control option
10.4.7 Determination of the temperature gradient in the sample
10.4.8 Advantages and disadvantages of parallel-plate measuring systems
10.5 Mooney/Ewart measuring systems (MEMS)
10.6 Relative measuring systems
10.6.1 Measuring systems with sandblasted, profiled or serrated surfaces
10.6.2 Spindles in the form of disks, pins, and spheres
10.6.3 Krebs spindles
10.6.4 Paste spindles and rotors showing pins and vanes
10.6.5 Ball measuring systems (motion along a circular path)
10.6.6 Further relative measuring systems
10.7 Measuring systems for solid torsion bars
10.7.1 Bars showing a rectangular cross section
10.7.2 Bars showing a circular cross section
10.7.3 Composite materials
10.8 Special measuring devices
10.8.1 Special measuring conditions which influence rheology
10.8.2 Rheo-optical measuring devices
10.8.3 Other special measuring devices
10.8.4 Other kinds of testings besides shear tests
10.9 References
11 Instruments
11.1 Introduction
11.2 Short overview: methods for testing viscosity and elasticity
11.2.1 Very simple determinations
11.2.2 Flow on a horizontal plane
11.2.3 Spreading or slump on a horizontal plane after lifting a container
11.2.4 Flow on an inclined plane
11.2.5 Flow on a vertical plane or over a special tool
11.2.6 Flow in a channel, trough or bowl
11.2.7 Flow cups and other pressureless capillary viscometers
11.2.8 Devices showing rising, sinking, falling and rolling elements
11.2.9 Penetrometers, consistometers and texture analyzers
11.2.10 Pressurized cylinder and capillary devices
11.2.11 Simple rotational viscometer tests
11.2.12 Devices with vibrating oroscillating elements
11.2.13 Rotational and oscillatory curemeters (for rubber testing)
11.2.14 Tension testers
11.2.15 Compression testers
11.2.16 Linear shear testers
11.2.17 Bending or flexure testers
11.2.18 Torsion testers
11.3 Flow cups
11.3.1 ISO cups
11.3.2 Other types of flow cups
11.4 Capillary viscometers
11.4.1 Glas scapillary viscometers
11.4.2 Pressurized capillary viscometers
11.5 Falling-ball viscometers
11.6 Stabinger viscometer
11.7 Rotational and oscillatory rheometers
11.7.1 Rheometer set ups
11.7.2 Controll oops
11.7.3 Devices to measure to
Standort:
Kompaktmagazin oben
Zweigbibliothek:
GFZ Bibliothek
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