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Open tubular columns prepared with very thick liquid phase film II. Investigations on column efficiency

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Abstract

The performance of a column prepared with an immobilized (chemically bonded) methylsilicone phase having a film thickness of 5μm is investigated in detail. Due to their high sample capacity, such columns are particularly useful when directly coupling gas chromatography with spectroscopic techniques such as Fourier-transform infrared spectroscopy. Thick-film columns can even be used with thermal conductivity detectors.

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Authors and Affiliations

  1. Chromatography Division, The Perkin-Elmer Corporation, 06856, Norwalk, Connecticut, U.S.A.

    L. S. Ettre & J. D. Walters

  2. Spectroscopy Division, The Perkin-Elmer Corporation, 06856, Norwalk, Connecticut, U.S.A.

    G. L. McClure

Authors
  1. L. S. Ettre
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  2. G. L. McClure
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  3. J. D. Walters
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Ettre, L.S., McClure, G.L. & Walters, J.D. Open tubular columns prepared with very thick liquid phase film II. Investigations on column efficiency. Chromatographia 17, 560–569 (1983). https://doi.org/10.1007/BF02261920

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  • DOI: https://doi.org/10.1007/BF02261920

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