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Microwave Assisted Deprotection of Trimethylsilyl Ethers under Solvent-Free Conditions Catalyzed by Clayor a Palladium Complex

Durch Ton oder einen Palladiumkomplex katalysierte mikrowellenunterstützte Entschützung von Trimethylsilylethern unter lösungsmittelfreien Bedingungen

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Summary.

 A simple method for the cleavage of trimethylsilyl ethers under microwave irradiation and solvent-free conditions in the presence of montmorillonite K-10 or a palladium complex catalyst in almost quantitative yield is reported.

Zusammenfassung.

 Eine einfache Methode zur Spaltung von Trimethylsilylethern unter Mikrowelleneinwirkung und lösungsmittelfreien Bedingungen in Gegenwart von Montmorillonit K-10 oder einem Palladiumkomplex mit nahezu quantitativen Ausbeuten wird beschrieben.

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Received September 28, 1998. Accepted (revised) December 1, 1998

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Mojtahedi, M., Saidi, M., Heravi, M. et al. Microwave Assisted Deprotection of Trimethylsilyl Ethers under Solvent-Free Conditions Catalyzed by Clayor a Palladium Complex. Monatshefte fuer Chemie 130, 1175–1178 (1999). https://doi.org/10.1007/PL00010296

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  • DOI: https://doi.org/10.1007/PL00010296

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