Summary.
A simple method for the cleavage of trimethylsilyl ethers under microwave irradiation and solvent-free conditions in the presence of montmorillonite K-10 or a palladium complex catalyst in almost quantitative yield is reported.
Zusammenfassung.
Eine einfache Methode zur Spaltung von Trimethylsilylethern unter Mikrowelleneinwirkung und lösungsmittelfreien Bedingungen in Gegenwart von Montmorillonit K-10 oder einem Palladiumkomplex mit nahezu quantitativen Ausbeuten wird beschrieben.
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Received September 28, 1998. Accepted (revised) December 1, 1998
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Mojtahedi, M., Saidi, M., Heravi, M. et al. Microwave Assisted Deprotection of Trimethylsilyl Ethers under Solvent-Free Conditions Catalyzed by Clayor a Palladium Complex. Monatshefte fuer Chemie 130, 1175–1178 (1999). https://doi.org/10.1007/PL00010296
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DOI: https://doi.org/10.1007/PL00010296