Skip to main content
SpringerLink
Log in

Gas-chromatographic characteristics of 2-methyl-2-propenyl alkyl sulfides

  • Published:
Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    The mass spectra were studied and the retention indices were determined on capillary columns with OV-101 and OV-17 phases under isothermal conditions at 130°C and with temperature programming for eight synthesized alkyl 2-methy1-2-propenyl sulfides.

  2. 2.

    Methods are proposed for the calculation of the retention indices of sulfur-containing compounds containing a 2-methyl-2-propenyl substituent. The retention indices for 32 substances (sulfides, disulfides, dithioformals) under isothermal conditions were predicted.

  3. 3.

    Equations are proposed for the calculation of the retention indices of the homologous series of n-alkyl 2-methyl-2-propenyl sulfides.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature cited

  1. S. Van Straten, F. de Vrijeer, and J. C. de Beauveser, Volatile Compounds in Foods, CIVO-TNO, Zeitst, The Netherlands (1977).

    Google Scholar 

  2. M. H. Brodnitz, J. V. Pascale, and L. V. Derslice, J. Agric. Food Chem.,19, 273 (1971).

    Google Scholar 

  3. R. V. Golovnya, V. G. Garbuzov, I. Ya. Grigor'eva (Grigorjeva), et al., Die Nahrung,26, 89 (1982).

    Google Scholar 

  4. R. G. Buttery, W. F. Haddon, R. M. Seifert, and J. G. Turnbangh. J. Agric. Food Chem.,32, 674 (1984).

    Google Scholar 

  5. M. Boelens, P. J. de Valois, H. J. Wobben, and A. Van der Gen, J. Agric. Food Chem.,19, 984 (1971).

    Google Scholar 

  6. R. V. Golovnya, T. A. Misharina, and V. G. Garbuzov, Izv. Akad. Nauk SSSR, Ser. Khim., 2539 (1978).

  7. R. V. Golovnya, T. A. Misharina, V. G. Garbuzov, and F. A. Medved'ev (Medvedyev), Die Nahrung,27, 237 (1983).

    PubMed  Google Scholar 

  8. T. A. Misharina, R. V. Golovnya, and S. V. Vitt, Prikl. Biokhim. Mikrobiol.,21, 107 (1985).

    Google Scholar 

  9. T. V. Mikhailova, A. I. Gren', L. E. Vysotskaya, et al., Zh. Anal. Khim.,40, 740 (1985).

    Google Scholar 

  10. Organic Chemistry. Practical Organic Chemistry [Russian translation], Vol. 1, Mir, Moscow (1979), pp. 279–280.

  11. E. E. Reid, Organic Chemistry of Bivalent Sulfur, Vol. 2, Chemical Publishing Company, New York (1960), pp. 16–19.

    Google Scholar 

  12. H. Van Der Dool and P. D. Kratz, J. Chromatogr.,11, 463 (1963).

    PubMed  Google Scholar 

  13. H. Budzikiewicz, C. Djerassi, and D. H. Williams, Interpretation of Mass Spectra in Organic Compounds, Holden-Day, San Francisco (1964).

    Google Scholar 

  14. V. G. Garbuzov, T. A. Misharina, A. F. Aérov, and R. V. Golovyna, Zh. Anal. Khim.,40, 709 (1985).

    Google Scholar 

  15. D. N. Grigor'eva, T. A. Misharina, and R. V. Golovnya, GKh Computer Algorithm for Identification of Sulfur-Containing Compounds in Complex Mixtures. Dumai Symposium on Chromatography. Abstracts [in Russian], Yalta (1985).

Download references

Author information

Authors and Affiliations

  1. A. N. Nesmeyanov Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, Moscow

    T. V. Mikhailova, T. A. Misharina, A. F. Aérov, V. A. Lyapin, A. I. Gren', L. E. Vysotskaya & R. V. Golovnya

  2. A. V. Bogat-skii Physicochemical Institute, Academy of Sciences of the Ukrainian SSR, Odessa

    T. V. Mikhailova, T. A. Misharina, A. F. Aérov, V. A. Lyapin, A. I. Gren', L. E. Vysotskaya & R. V. Golovnya

Authors
  1. T. V. Mikhailova
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. T. A. Misharina
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. A. F. Aérov
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. V. A. Lyapin
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. A. I. Gren'
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. L. E. Vysotskaya
    View author publications

    You can also search for this author in PubMed Google Scholar

  7. R. V. Golovnya
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 7, pp. 1525–1529, July, 1987.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Mikhailova, T.V., Misharina, T.A., Aérov, A.F. et al. Gas-chromatographic characteristics of 2-methyl-2-propenyl alkyl sulfides. Russ Chem Bull 36, 1407–1410 (1987). https://doi.org/10.1007/BF01557512

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01557512

Keywords

Search

Navigation