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Obtaining and sintering yttria stabilized zirconia (YSZ) powders from alkoxides

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Abstract

Amorphous zirconia ceramics powders containing 3 and 6 mol% yttria were prepared by controlled hydrolysis of alkoxides. Characterization of these powders was carried away by Thermal Analysis, X-ray Diffraction, Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Analysis (EDAX™). The calcination temperature was optimized for compaction at a temperature ranging from 500–800°C. 3% molar YSZ powders from alkoxide, that attained 98% of the theoretical bulk density, showed the best behaviour.

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Authors and Affiliations

  1. Departamento de Estructura y Propiedades de los Materiales, Facultad de Ciencias, Universidad de Cádiz, Apartado 40, Puerto Real, 11510, Cádiz, Spain

    C. Barrera-Solano, C. Jiménez-Solís, N. de la Rosa-Fox & L. Esquivias

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  1. C. Barrera-Solano
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  2. C. Jiménez-Solís
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  3. N. de la Rosa-Fox
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  4. L. Esquivias
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Barrera-Solano, C., Jiménez-Solís, C., de la Rosa-Fox, N. et al. Obtaining and sintering yttria stabilized zirconia (YSZ) powders from alkoxides. J Sol-Gel Sci Technol 2, 347–352 (1994). https://doi.org/10.1007/BF00486268

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  • DOI: https://doi.org/10.1007/BF00486268

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