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High temperature 1H NMR studies of epoxy cure: A neglected technique

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Summary

By reference to the reaction of a copper complex of phenyl glycidyl ether and 2-ethyl-4-methylimidazole, and Bisphenol A diglycidyl ether, 1H nuclear magnetic resonance spectroscopy at high temperature is shown to be an excellent and under-utilized method for measuring the degree of cure, enabling kinetic parameters to be obtained.

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References

  1. Buist GJ, Hagger AJ, Howlin BJ, Jones, JR, Parker MJ, Barton JM and Wright WW (1993) Computers and Chemistry, 7: 257

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  2. Ashcroft WR (1993) Curing agents for epoxy resins, Chapter 2 in Chemistry and Technology of Epoxy Resins Ellis B (Ed) Blackie Academic and Professional, Glasgow and London, p 58

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  6. Barton JM, Buist GJ, Hamerton I, Howlin BJ, Jones, JR and Liu S (1994) Development of Novel Epoxy Curing Agents. 2. Comparative kinetic analyses for epoxy resins cured with imidazole-metal complexes, in preparation

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Authors and Affiliations

  1. Materials and Structures Department, Defence Research Agency, GU14 6TD, Farnborough, Hampshire, UK

    John M. Barton

  2. Department of Chemistry, University of Surrey, GU2 5XH, Guildford, Surrey, UK

    Gabriel J. Buist, Ian Hamerton, Brendan J. Howlin, John R. Jones & Shuyuan Liu

Authors
  1. John M. Barton
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  2. Gabriel J. Buist
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  3. Ian Hamerton
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  4. Brendan J. Howlin
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  5. John R. Jones
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  6. Shuyuan Liu
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Barton, J.M., Buist, G.J., Hamerton, I. et al. High temperature 1H NMR studies of epoxy cure: A neglected technique. Polymer Bulletin 33, 215–219 (1994). https://doi.org/10.1007/BF00297358

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  • DOI: https://doi.org/10.1007/BF00297358

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