Summary
A technique is described, which permits obtaining the correct weight of a volatile substance, vapor pressure not exceeding four atmospheres at ambient temperature, previous to combustion in a vacuum system.
Zusammenfassung
Eine Arbeitsweise wird beschrieben, um flüchtige Stoffe mit weniger als vier Atmosphären Dampfdruck bei gewöhnlicher Temperatur vor der Verbrennung in einer Vakuumapparatur zu wägen.
Résumé
On décrit une technique qui permet d'obtenir le poids correct d'une substance volatile, la pression de vapeur n'excédant pas 4 atmosphéres á température ambiante, avant la combustion sous vide.
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Literature
J. W. Frazer, Lawrence Radiation Laboratory (Livermore) Report UCRL-5134 (1958).
J. W. Frazer, Mikrochim. Acta [Wien]1962, 993.
J. W. Frazer andR. W. Crawford, Mikrochim. Acta [Wien]1963, 561.
E. B. Bissell andD. B. Fields, J. Org. Chem., in process.
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This work was performed under the auspices of the U. S. Atomic Energy Commission.
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Frazer, J.W., Crawford, R.W. The handling of volatile compounds for the simultaneous determination of carbon, hydrogen, and nitrogen. Mikrochim Acta 52, 676–678 (1964). https://doi.org/10.1007/BF01215711
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DOI: https://doi.org/10.1007/BF01215711