Abstract
Several artificial rainwater samples and a natural sample of road dust have been analysed for trimethyllead under the aegis of a European Union Measurement and Testing (Bureau of Community Reference — BCR) intercomparison exercise, using a new and simplified purge and trap ethylation technique. Levels of trimethyllead found have been similar to those reported at lower levels from the natural environment. The method has been successful in the presence of excess amounts of inorganic lead, even for organic lead levels one tenth of those recently reported for the natural environment.
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Van Cleuvenbergen RJ, Adams FC (1992) Environ Sci Technol 26:1354
Turnbull AB, Wang Y, Harrison RM (1993) Appl Organomet Chem 7:567
Department of the Environment (UK) (1993) Digest of Environmental Protection and Water Statistics, No 15, 1992. HMSO London
Radojevic M, Harrison RM (1987) Atmos Environ 21:2403
Page RA, Cawse PA, Baker S (1988) Sci Total Environ 68:71
Witte C, Szpunar-Lobinska J, Lobinski R, Adams FC (1994) Appl Organomet Chem 8:in press
Stang MP, Seligman PF (1986) Chemosphere 15:1256
Martin F (1993) Thèse, Université de Bordeaux I, France (Développement des Methodes Analytiques. Thèse No 1024)
Honeycutt JB, Riddle JM (1960) J Amer Chem Soc 82:3051 (and refs therein)
Rapsomanikis S, Donard OFX, Weber JH (1986) Anal Chem 58:35
Bloom N (1989) Can J Fish Aquat Sci 46:1131
Rapsomanikis S, Craig PJ (1991) Anal Chim Acta 298:563
Clark S, Craig PJ (1992) Microchim Acta 109:141
Mennie D (1993) PhD Thesis, De Montfort University, Leicester, UK (Novel methods for the analysis of organometallic compounds in the environment)
Edbon L, Goodall P, Hill SJ, Stockwell P, Thompson KC (1993) J Anal At Spectrom 8:723
Clamagirand V, Marr IL, Wardell JL (1993) Appl Organomet Chem 7:577
Ashby JR, Craig PJ (1989) Sci Total Environ 78:219
Ashby JR, Craig PJ (1991) Appl Organomet Chem 5:173
Sturgeon RE, Willie SN, Berman SS (1989) Anal Chem 61:1867
Craig PJ, Garraud H, Laurie SH, Mennie D, Stojak GH (1994) J Organomet Chem 468:7 (and refs therein)
Blais JS, Marshall WD (1989) J Anal Spectrom 4:641
Lobinski R, Adams FC (1992) Anal Chim Acta: 262:285
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Craig, P.J., Dewick, R.J. & van Elteren, J.T. Use of sodium tetraethylborate for the analysis of trimethyllead species in artificial rainwater and a natural road dust sample. Fresenius J Anal Chem 351, 467–470 (1995). https://doi.org/10.1007/BF00322921
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DOI: https://doi.org/10.1007/BF00322921