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Simultaneous comparison of δ31P and 1JPN for the assignment of E/Z-stereochemistry of the phosphorus-nitrogen double bond in iminophosphines R-P=N-R′

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Abstract

 The analysis of 31P and 15N NMR data of a series of 40 iminophosphines R-P=N-R′ reveals that the E/Z-stereochemistry of the PN double bond can be predicted on the basis of a simultaneous comparison of the values of δ31P and 1JPN.

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Authors and Affiliations

  1. Institut für Anorganische Chemie der Universität, Gerhard-Domagk-Strasse 1, D-53121 Bonn, Germany, , , , , , DE

    D. Gudat & E. Niecke

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  1. D. Gudat
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  2. E. Niecke
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Received: 31 May 1996/Revised: 2 July 1996/Accepted: 5 July 1996

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Gudat, D., Niecke, E. Simultaneous comparison of δ31P and 1JPN for the assignment of E/Z-stereochemistry of the phosphorus-nitrogen double bond in iminophosphines R-P=N-R′. Fresenius J Anal Chem 357, 482–484 (1997). https://doi.org/10.1007/s002160050196

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  • DOI: https://doi.org/10.1007/s002160050196

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