Crystal structure and spectroscopic study of [Cu(BPCA)(OH2)(O2CCH3)·H2O complex; BPC = N-2-pyridinylcarbonyl-2-pyridinecarboximidate anion
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Syntheses, structures and properties of structurally characterised complexes of imide-based ligands
2012, Coordination Chemistry ReviewsCitation Excerpt :The crystal packing of these complexes often shows head to tail carbonyl–carbonyl interactions [60], stacking of pyridine rings [27,61] and extensive hydrogen bonding networks between the imide oxygen atoms and coordinated and uncoordinated solvent molecules (Fig. 17) [58,59,61,62]. An unusual feature is present in the crystal packing of [CuII(bpca)(H2O)2](NO3)·2H2O [57] and [CuII(bpca)(3ClC6H4CO2)] [61]. In [CuII(bpca)(H2O)2](NO3)·2H2O, in the sixth potential coordination site of the copper(II) centre, a very weak side-on interaction (3.302 Å) occurs with the imide oxygen atom of an adjacent complex.
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