Ring size control in diorganotin sulphides by intramolecular SnN coordination
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Hemi Labile Intramolecular N → Sn Coordination in a Diorganotin (IV) Sulfide [R<inf>2</inf>Sn(µ-S)]<inf>2</inf> (R = 2-phenylazophenyl) Complex: Synthesis, Structure, DFT-NBO and Antibacterial Studies
2021, PolyhedronCitation Excerpt :When the N2 centre, being a Lewis base, attacks the Lewis acidic Sn1 center over the face C1C13S1, the axial Sn1-S1ʹ bond gets elongated in comparison to the axial Sn1-S1 bond [Fig. 1(c)]. The complex 1 has an Sn2S2 ring with an Sn1-S1 distance of 2.4007 Å and Sn1-S1ʹ distance of 2.4761 Å, which are in close agreement with previous reports on [R2Sn(µ-S)]2 rings bearing N → Sn intramolecular coordination. [24] Also, these bond parameters are much closer to the four membered Sn2S2 ring (Sn-S, 2.4001, 2.4817 Å and Sn-S-Sn, 86.79°) of our previously reported tetranuclear double decker compopund [(RSn)4(µ-S)6] (R = 2-phenylazophenyl). [9]
Reactivity of a C,N-chelated stannylene with chalcogens
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