High-performance liquid chromatography of alkyl phosphite-substituted derivatives of iron pentacarbonyl

Journal of Chromatography A

Volume 265, 1983, Pages 347-352

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The chromatographic behaviour of some monosubstituted derivatives of the tetranuclear cluster (Cp)NiOs₃ (μH)₃(CO)₉ (Cp = cyclopentadienyl) with group V donor ligands (benzonitrile tertiary phosphines, triphenylamine and triphenylstibine) is reported. In reversed-phase and adsorption liquid chromatography, the kind of the substituents strongly influences the retention volumes, the dimension of the whole cluster having less effect. Correlations of retention volumes with the nature of the substituents were found only for small of compounds.
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