Skip to main content
SpringerLink
Log in

Quantitative fluorodensitometric determination of ergot alkaloids

II. Determination of hydrogenated ergot alkaloids of the ergotoxine group

  • Originals
  • Published:
Chromatographia Aims and scope Submit manuscript

Summary

A direct fluorodensitometric method for the quantitative measurement of the dihydroalkaloids of the ergotoxine group, after separation by thin-layer chromatography, is described. The absorption and excitation spectra of dihydroergocristine, dihydroergocornine, and dihydroergocryptine were recorded. The linear range between peak area and concentration is given. Under selected conditions the relative fluoresence, intensities were determined.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. M. Prošek, E. Kučan, M. Katić, M. Bano, Chromatographia9, 273 (1976).

    Google Scholar 

  2. C. Galeffi, E. M. Delle Monache, J. Chromatogr.88, 413 (1974).

    Google Scholar 

  3. A. Stoll, A. Rüegger, Helv. Chim. Acta37, 1725 (1954).

    Google Scholar 

  4. F. Adamanis, E. Pawelozyk, Z. Plotkowiakowa, Bull. Soc. Amis Sci. Lett. Pozman C10, 95 (1960).

    Google Scholar 

  5. Z. Gawrych, J. Wilczynska, Acta Pol. Pharm.22, 1 (1965).

    Google Scholar 

  6. M. zinser, Ch. Baumgaertel, Arch. Pharm.297, 158 (1964).

    Google Scholar 

  7. E. Roeder, E. Mutschler, H. Rochelmeyer Z. Anal. Chem.244, 46 (1969).

    Google Scholar 

  8. L. Wichlinski, Acta Pol. Pharm.26, 617 (1969).

    Google Scholar 

  9. H. Rochelmeyer, E. Stahl, A. Patani, Arch. Pharmaz.291, 1 (1958).

    Google Scholar 

  10. T. Hohmann, H. Rochelmeyer, Arch. Pharmaz.297, 186 (1964).

    Google Scholar 

  11. R. A. Heacock, K. R. Langille, J. D. MacNeil, R. W. Frei, J. Chromatogr77, 425 (1973).

    Google Scholar 

  12. K. Teichert, E. Mutschler, H. Rochelmeyer, Dtsch. Apotheker Zt.100, 283 (1960).

    Google Scholar 

  13. K. C. Guven, L. Eroglu, Eczacilik Bul.10/4, 53 (1958).

    Google Scholar 

  14. R. Fowler, P. J. Gomm, D. A. Patterson, J., Chromatogr.72, 351 (1972).

    Google Scholar 

  15. K. Macek, J. Vecerkova, Pharmazie20/10, 605 (1965).

    Google Scholar 

  16. P. Heinänen, M. Järvi, M. Lähteenmäki, Farm. Aikakaislehti68, 155 (1959).

    Google Scholar 

  17. S. Keipert, R. Voigt, J. Chromatogr.72, 327 (1972).

    Google Scholar 

  18. K. Röder, E. Mutschler H. Rochelmeyer, Pharm. Acta Helv.42, 402 (1967).

    Google Scholar 

  19. V. Prochazka, F. Kavka, M. Prucha, J. Pitra, Ceskoslov. Farm.14, 154 (1965).

    Google Scholar 

  20. M. Vanhaelen, R. Vanhaelen-Fastre, J. Chromatogr.72, 139 (1972).

    Google Scholar 

  21. C.J.G.A. Bos, J.M.G.J. Frijns, Pharm. Weekblad107, 111 (1972).

    Google Scholar 

  22. J.M.G.J. Frijns Pharm. Weekblad105, 709 (1970).

    Google Scholar 

  23. J.M.G.J. Frijns, Pharm. Weekblad.106, 865 (1971).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Analytical Laboratory, LEK Pharmaceutical and Chemical Works, Celovška 135, 61000, Ljubljana, Yugoslavia

    M. Prosěk, E. Kučan, M. Katić & M. Bano

Authors
  1. M. Prosěk
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. E. Kučan
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. M. Katić
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. M. Bano
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

For Part I, see ref. [1]

Rights and permissions

Reprints and permissions

About this article

Cite this article

Prosěk, M., Kučan, E., Katić, M. et al. Quantitative fluorodensitometric determination of ergot alkaloids. Chromatographia 9, 325–327 (1976). https://doi.org/10.1007/BF02268835

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02268835

Keywords

Search

Navigation